(3S,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Base Information

Chemical Name:(3S,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal
CAS No.:566949-72-2
Molecular Formula:C₃₁H₅₈O₅Si₂
Molecular Weight:566.97
Hs Code.:

Synonyms:(3S,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

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Chemical Property of (3S,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Chemical Property:

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Technology Process of (3S,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

There total 8 articles about (3S,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 566949-72-2
(3S,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

2: 57 percent / LiBH₄ / methanol; tetrahydrofuran / 16 h / 20 °C

3: 75 percent / imidazole / dimethylformamide / 1.5 h / 60 °C

4: aq. OsO₄; NMO / acetone; 2-methyl-propan-2-ol / 16 h / 20 °C

5: 0.59 g / NaIO₄ / methanol / 1 h / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; lithium borohydride; N-methyl-2-indolinone; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1039/b211801g

Reference yield:

: (4S,5S)-5-(3,4-Dimethoxy-phenyl)-5-triisopropylsilanyloxy-4-triisopropylsilanyloxymethyl-pentane-1,2-diol

: 566949-72-2
(3S,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Guidance literature:: With sodium periodate; In methanol; at 20 ℃; for 1h;
DOI:10.1039/b211801g

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 566949-72-2
(3S,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / imidazole / dimethylformamide / 1.5 h / 60 °C

2: aq. OsO₄; NMO / acetone; 2-methyl-propan-2-ol / 16 h / 20 °C

3: 0.59 g / NaIO₄ / methanol / 1 h / 20 °C

With 1H-imidazole; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; In methanol; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1039/b211801g