(1R,3R,5S,6R,7R,8S,9R)-2-allyl-6,7-di-O-benzyl-3-methyl-9-nitro-3,8-oxy-2-azabicyclo[3.3.1]nonane

Base Information

Chemical Name:(1R,3R,5S,6R,7R,8S,9R)-2-allyl-6,7-di-O-benzyl-3-methyl-9-nitro-3,8-oxy-2-azabicyclo[3.3.1]nonane
CAS No.:1198581-93-9
Molecular Formula:C₂₆H₃₀N₂O₅
Molecular Weight:450.535
Hs Code.:

Synonyms:(1R,3R,5S,6R,7R,8S,9R)-2-allyl-6,7-di-O-benzyl-3-methyl-9-nitro-3,8-oxy-2-azabicyclo[3.3.1]nonane

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Chemical Property of (1R,3R,5S,6R,7R,8S,9R)-2-allyl-6,7-di-O-benzyl-3-methyl-9-nitro-3,8-oxy-2-azabicyclo[3.3.1]nonane

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Technology Process of (1R,3R,5S,6R,7R,8S,9R)-2-allyl-6,7-di-O-benzyl-3-methyl-9-nitro-3,8-oxy-2-azabicyclo[3.3.1]nonane

There total 3 articles about (1R,3R,5S,6R,7R,8S,9R)-2-allyl-6,7-di-O-benzyl-3-methyl-9-nitro-3,8-oxy-2-azabicyclo[3.3.1]nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1198582-02-3
C₂₃H₂₅NO₆

: 107-11-9,30551-89-4
1-amino-2-propene

: 1198581-93-9
(1R,3R,5S,6R,7R,8S,9R)-2-allyl-6,7-di-O-benzyl-3-methyl-9-nitro-3,8-oxy-2-azabicyclo[3.3.1]nonane

: (1S,5R,6R,7R,8R,9S)-2-allyl-6,7-di-O-benzyl-8-hydroxy-3-methyl-9-nitro-2-azabicyclo[3.3.1]nonan-3-ene

Guidance literature:: C₂₃H₂₅NO₆; With sodium methylate; In methanol; at 20 ℃; for 2h;

1-amino-2-propene; In methanol; at 20 ℃; for 48h;
DOI:10.1016/j.carres.2009.08.028

Reference yield: 19.0%

: 1198581-96-2
(1S,2R,3R,4R,5R,6S)-1-acetylmethyl-2,3-di-O-benzyl-4-hydroxy-5-methoxy-6-nitrocyclohexane

: 107-11-9,30551-89-4
1-amino-2-propene

: 1198581-93-9
(1R,3R,5S,6R,7R,8S,9R)-2-allyl-6,7-di-O-benzyl-3-methyl-9-nitro-3,8-oxy-2-azabicyclo[3.3.1]nonane

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 2h;
DOI:10.1016/j.carres.2009.08.028

Reference yield:

: 1198582-02-3
C₂₃H₂₅NO₆

: 107-11-9,30551-89-4
1-amino-2-propene

: 1198581-93-9
(1R,3R,5S,6R,7R,8S,9R)-2-allyl-6,7-di-O-benzyl-3-methyl-9-nitro-3,8-oxy-2-azabicyclo[3.3.1]nonane

: (1S,3S,5R,6R,7R,8R,9S)-2-allyl-6,7-di-O-benzyl-8-hydroxy-3-methyl-9-nitro-2-azabicyclo[3.3.1]nonane

Guidance literature:: C₂₃H₂₅NO₆; With sodium methylate; In methanol; at 20 ℃; for 2h;

1-amino-2-propene; With sodium cyanoborohydride; In methanol; at 20 ℃; for 16h;
DOI:10.1016/j.carres.2009.08.028