triethyl cis,cis,cis-2,5,8-tris(4-bromobenzyl)trindane-2,5,8-tricarboxylate

Base Information

Chemical Name:triethyl cis,cis,cis-2,5,8-tris(4-bromobenzyl)trindane-2,5,8-tricarboxylate
CAS No.:1003321-28-5
Molecular Formula:C₄₅H₄₅Br₃O₆
Molecular Weight:921.561
Hs Code.:

Synonyms:triethyl cis,cis,cis-2,5,8-tris(4-bromobenzyl)trindane-2,5,8-tricarboxylate

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Chemical Property of triethyl cis,cis,cis-2,5,8-tris(4-bromobenzyl)trindane-2,5,8-tricarboxylate

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Technology Process of triethyl cis,cis,cis-2,5,8-tris(4-bromobenzyl)trindane-2,5,8-tricarboxylate

There total 1 articles about triethyl cis,cis,cis-2,5,8-tris(4-bromobenzyl)trindane-2,5,8-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 589-15-1
1-bromomethyl-4-bromobenzene

: 410074-24-7
triethyl trindane-2,5,8-tricarboxylate

: 1003321-29-6
triethyl cis,trans,trans-2,5,8-tris(4-bromobenzyl)trindane-2,5,8-tricarboxylate

: 1003321-28-5
triethyl cis,cis,cis-2,5,8-tris(4-bromobenzyl)trindane-2,5,8-tricarboxylate

Guidance literature:: triethyl trindane-2,5,8-tricarboxylate; With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -90 ℃;

1-bromomethyl-4-bromobenzene; In tetrahydrofuran; n-heptane; ethylbenzene; at -90 ℃; Further stages.;
DOI:10.1055/s-2007-990828

Reference yield: 67.0%

: 1003321-28-5
triethyl cis,cis,cis-2,5,8-tris(4-bromobenzyl)trindane-2,5,8-tricarboxylate

: 1003321-30-9
triethyl cis,cis,cis-2,5,8-tris(4-aminobenzyl)trindane-2,5,8-tricarboxylate

Guidance literature:: With tri-tert-butyl phosphine; lithium hexamethyldisilazane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; at 50 ℃; for 48h;
DOI:10.1055/s-2007-990828