7-(4-biphenyl)-1-(2-deoxy-3,5-di-O-p-toluoyl-α-D-ribofuranosyl)lumazine

Base Information

Chemical Name:7-(4-biphenyl)-1-(2-deoxy-3,5-di-O-p-toluoyl-α-D-ribofuranosyl)lumazine
CAS No.:170158-06-2
Molecular Formula:C₃₉H₃₂N₄O₇
Molecular Weight:668.706
Hs Code.:

Synonyms:7-(4-biphenyl)-1-(2-deoxy-3,5-di-O-p-toluoyl-α-D-ribofuranosyl)lumazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(4-biphenyl)-1-(2-deoxy-3,5-di-O-p-toluoyl-α-D-ribofuranosyl)lumazine

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Technology Process of 7-(4-biphenyl)-1-(2-deoxy-3,5-di-O-p-toluoyl-α-D-ribofuranosyl)lumazine

There total 2 articles about 7-(4-biphenyl)-1-(2-deoxy-3,5-di-O-p-toluoyl-α-D-ribofuranosyl)lumazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4974-58-7
4-biphenylglyoxal

: 170158-06-2
7-(4-biphenyl)-1-(2-deoxy-3,5-di-O-p-toluoyl-α-D-ribofuranosyl)lumazine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / aq. NH₃; ethanol / 2 h / Heating

2: 1.) HMDS, chlorotrimethylsilylmethane, 2.) ZnCl₂ / 1.) acetonitrile, 2.) -25 deg C, dichloromethane

With 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; Chloromethyltrimethylsilane; In ammonium hydroxide; ethanol;
DOI:10.1080/07328319608002396

Reference yield:

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 170157-98-9
7-(4-biphenyl)lumazine

: 170158-02-8
7-(4-biphenyl)-1-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)lumazine

: 170158-06-2
7-(4-biphenyl)-1-(2-deoxy-3,5-di-O-p-toluoyl-α-D-ribofuranosyl)lumazine

Guidance literature:: With 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; Chloromethyltrimethylsilane; Yield given. Multistep reaction. Yields of byproduct given; 1.) acetonitrile, 2.) -25 deg C, dichloromethane;
DOI:10.1080/07328319608002396