C₄₀H₅₃NO₇

Base Information

Chemical Name:C₄₀H₅₃NO₇
CAS No.:1265221-67-7
Molecular Formula:C₄₀H₅₃NO₇
Molecular Weight:659.863
Hs Code.:

C<sub>40</sub>H<sub>53</sub>NO<sub>7</sub>

Synonyms:C₄₀H₅₃NO₇

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Chemical Property of C₄₀H₅₃NO₇

Chemical Property:

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Technology Process of C₄₀H₅₃NO₇

There total 17 articles about C₄₀H₅₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1265221-66-6
C₄₃H₅₃NO₁₀

: 1265221-67-7
C₄₀H₅₃NO₇

: 1265221-68-8
C₄₂H₅₁NO₁₀

Guidance literature:: C₄₃H₅₃NO₁₀; With water; potassium hydroxide; at 130 ℃; for 4h; Inert atmosphere;

With toluene-4-sulfonic acid; In toluene; for 0.5h; Molecular sieve; Reflux;
DOI:10.1002/ejoc.201001133

Reference yield:

: 1016650-10-4
2-(3-isopropoxy-4-methoxyphenyl)ethanol

: 1265221-67-7
C₄₀H₅₃NO₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 18 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / tetrahydrofuran; water / 1.5 h / 90 °C / Inert atmosphere; Microwave irradiation

3.1: water; potassium hydroxide / 4 h / 130 °C / Inert atmosphere

3.2: 0.5 h / Molecular sieve; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; tetrabutylammomium bromide; water; potassium carbonate; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; water; 1.1: Mitsunobu reaction / 2.1: Suzuki coupling;
DOI:10.1002/ejoc.201001133

Reference yield:

: 1265221-59-7
2-(3,4-diisopropoxyphenoxy)tetrahydro-2H-pyran

: 1265221-67-7
C₄₀H₅₃NO₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-Bromosuccinimide; sodium carbonate / N,N-dimethyl-formamide / 3 h / 0 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 12.66 h / -78 - 18 °C / Inert atmosphere

3.1: hydrogenchloride; water / tetrahydrofuran; hexane / 0.25 h

3.2: 24 h

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / tetrahydrofuran; water / 1 h / 60 °C / Inert atmosphere; Microwave irradiation

5.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 14 h / 18 °C

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 18 °C

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / tetrahydrofuran; water / 1.5 h / 90 °C / Inert atmosphere; Microwave irradiation

8.1: water; potassium hydroxide / 4 h / 130 °C / Inert atmosphere

8.2: 0.5 h / Molecular sieve; Reflux

With hydrogenchloride; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; di-isopropyl azodicarboxylate; tetrabutylammomium bromide; water; sodium carbonate; potassium carbonate; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; hexane; water; N,N-dimethyl-formamide; 6.1: Mitsunobu reaction / 7.1: Suzuki coupling;
DOI:10.1002/ejoc.201001133