di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4,5-dimethoxyphenyl)fluorosilane

Base Information

Chemical Name:di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4,5-dimethoxyphenyl)fluorosilane
CAS No.:1396506-69-6
Molecular Formula:C₂₃H₄₃FO₃Si₂
Molecular Weight:442.762
Hs Code.:

Synonyms:di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4,5-dimethoxyphenyl)fluorosilane

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Chemical Property of di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4,5-dimethoxyphenyl)fluorosilane

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Technology Process of di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4,5-dimethoxyphenyl)fluorosilane

There total 3 articles about di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4,5-dimethoxyphenyl)fluorosilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1396506-59-4
(5-bromo-2,3-dimethoxybenzyloxy)(tert-butyl)dimethylsilane

: 558-63-4
di-tert-butyldifluorosilane

: 1396506-69-6
di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4,5-dimethoxyphenyl)fluorosilane

Guidance literature:: (5-bromo-2,3-dimethoxybenzyloxy)(tert-butyl)dimethylsilane; With tert.-butyl lithium; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.0833333h;

di-tert-butyldifluorosilane; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 19h;
DOI:10.3390/molecules16097458

Reference yield:

: 71295-21-1
5-bromo-2,3-dimethoxybenzaldehyde

: 1396506-69-6
di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4,5-dimethoxyphenyl)fluorosilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / methanol; water / 24 h / 20 °C

2.1: 1H-imidazole / dichloromethane / 20 h / 20 °C

3.1: tert.-butyl lithium / tetrahydrofuran; diethyl ether / 0.08 h / -78 °C

3.2: 19 h / -78 - 20 °C

With 1H-imidazole; sodium tetrahydroborate; tert.-butyl lithium; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.3390/molecules16097458

Reference yield:

: 86232-34-0
(5-bromo-2,3-dimethoxyphenyl)methanol

: 1396506-69-6
di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4,5-dimethoxyphenyl)fluorosilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / dichloromethane / 20 h / 20 °C

2.1: tert.-butyl lithium / tetrahydrofuran; diethyl ether / 0.08 h / -78 °C

2.2: 19 h / -78 - 20 °C

With 1H-imidazole; tert.-butyl lithium; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.3390/molecules16097458