[C(CF₃)2((2,6-(3,5-(CF₃)2C₆H₃)2-4-yl-C₆H₂)-N=C(H)-(3,5-(3,5-(CF₃)2C₆H₃)2-2-(OH)-C₆H₂))2]

Base Information

• Chemical Name: [C(CF₃)2((2,6-(3,5-(CF₃)2C₆H₃)2-4-yl-C₆H₂)-N=C(H)-(3,5-(3,5-(CF₃)2C₆H₃)2-2-(OH)-C₆H₂))2]
• CAS No.: 1198089-44-9
• Molecular Formula: C₉₃H₃₆F₅₄N₂O₂
• Molecular Weight: 2239.23

Synonyms:[C(CF₃)2((2,6-(3,5-(CF₃)2C₆H₃)2-4-yl-C₆H₂)-N=C(H)-(3,5-(3,5-(CF₃)2C₆H₃)2-2-(OH)-C₆H₂))2]

Chemical Property of [C(CF₃)2((2,6-(3,5-(CF₃)2C₆H₃)2-4-yl-C₆H₂)-N=C(H)-(3,5-(3,5-(CF₃)2C₆H₃)2-2-(OH)-C₆H₂))2]

Chemical Property:

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Technology Process of [C(CF₃)2((2,6-(3,5-(CF₃)2C₆H₃)2-4-yl-C₆H₂)-N=C(H)-(3,5-(3,5-(CF₃)2C₆H₃)2-2-(OH)-C₆H₂))2]

There total 1 articles about [C(CF₃)2((2,6-(3,5-(CF₃)2C₆H₃)2-4-yl-C₆H₂)-N=C(H)-(3,5-(3,5-(CF₃)2C₆H₃)2-2-(OH)-C₆H₂))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4'-hydroxy-3,5,3'',5''-tetrakis-trifluoromethyl-[1,1';3',1'']terphenyl-5'-carbaldehyde + C47H20F30N2 (1198089-41-6) → [C(CF3)2((2,6-(3,5-(CF3)2C6H3)2-4-yl-C6H2)-N=C(H)-(3,5-(3,5-(CF3)2C6H3)2-2-(OH)-C6H2))2] (1198089-44-9)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 80 ℃; for 12h; Inert atmosphere; Azeotropic water removal;

DOI:10.1039/b912883b

Reference yield: 77.0%

(pyridine)2Ni(CH3)2 (632326-69-3) + [C(CF3)2((2,6-(3,5-(CF3)2C6H3)2-4-yl-C6H2)-N=C(H)-(3,5-(3,5-(CF3)2C6H3)2-2-(OH)-C6H2))2] (1198089-44-9) → [C(CF3)2([2,6-(3,5-(CF3)2C6H3)2-4-yl-C6H2)-N=C(H)-(3,5-(3,5-(CF3)2C6H3)2-2-O-C6H2)-κ2-N,O[Ni(CH3)(pyridine))2]

Guidance literature:

In diethyl ether; byproducts: CH4; under inert atm., Schlenk techniques; cold Et2O added to mixt. of nickelcomplex and bis(salicylaldimine) under stirring, mixt. stirred at 25.de gree.C for ca. 150 min; evapn. under vac., residue dissolved in benzene, soln. filtered through syringe filter, volatiles removed by sublimation at -10°C and 1E-3 mbar;, elem. anal.;

DOI:10.1039/b912883b

upstream raw materials:

C₄₇H₂₀F₃₀N₂

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