C₁₄H₁₈F₂O₂

Base Information

Chemical Name:C₁₄H₁₈F₂O₂
CAS No.:1314964-79-8
Molecular Formula:C₁₄H₁₈F₂O₂
Molecular Weight:256.293
Hs Code.:

C<sub>14</sub>H<sub>18</sub>F<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₄H₁₈F₂O₂

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Chemical Property of C₁₄H₁₈F₂O₂

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Technology Process of C₁₄H₁₈F₂O₂

There total 6 articles about C₁₄H₁₈F₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 220437-02-5
4-(2,3-difluoro-4-ethoxyphenyl)-cyclohexanone

: 1314964-79-8
C₁₄H₁₈F₂O₂

Guidance literature:: 4-(2,3-difluoro-4-ethoxyphenyl)-cyclohexanone; With lithium aluminium tetrahydride; In N,N-dimethyl-formamide; at 20 ℃; for 5h; Cooling with ice;

With hydrogenchloride; In water; N,N-dimethyl-formamide; Cooling with ice;

Reference yield:

: 144292-32-0
2,3-difluoro-4-bromophenol

: 1314964-79-8
C₁₄H₁₈F₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide; tetrabutylammomium bromide / water / 6 h / 80 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 2 h / -70 °C / Inert atmosphere

2.2: 16 h / 20 °C

3.1: toluene-4-sulfonic acid / toluene / 4 h / Reflux

4.1: hydrogen / palladium on activated charcoal / isopropyl alcohol / 6 h / 20 °C

5.1: formic acid / toluene / 4 h / Reflux

6.1: lithium aluminium tetrahydride / N,N-dimethyl-formamide / 5 h / 20 °C / Cooling with ice

6.2: Cooling with ice

With lithium aluminium tetrahydride; n-butyllithium; formic acid; tetrabutylammomium bromide; hydrogen; toluene-4-sulfonic acid; sodium hydroxide; palladium on activated charcoal; In tetrahydrofuran; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene;

Reference yield:

: 220436-96-4
8-(4-ethoxy-2,3-difluorophenyl)-1,4-dioxaspiro[4.5]decane-8-ol

: 1314964-79-8
C₁₄H₁₈F₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 4 h / Reflux

2.1: hydrogen / palladium on activated charcoal / isopropyl alcohol / 6 h / 20 °C

3.1: formic acid / toluene / 4 h / Reflux

4.1: lithium aluminium tetrahydride / N,N-dimethyl-formamide / 5 h / 20 °C / Cooling with ice

4.2: Cooling with ice

With lithium aluminium tetrahydride; formic acid; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In N,N-dimethyl-formamide; isopropyl alcohol; toluene;