Technology Process of C46H38BF2N3S2
There total 5 articles about C46H38BF2N3S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,7-dithienyl-3,5-di(4-bromophenyl)borondifluoride-azadipyrromethene; mesitylboronic acid;
With
sodium carbonate;
In
tetrahydrofuran; water; toluene;
for 0.0833333h;
Inert atmosphere;
With
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; water; toluene;
at 80 ℃;
DOI:10.1002/ejoc.201301300
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: methanol / Reflux
2.1: ammonium acetate / butan-1-ol / 120 °C
3.1: N-ethyl-N,N-diisopropylamine / chloroform / 1 h
3.2: 20 °C
4.1: sodium carbonate / water; tetrahydrofuran; toluene / 0.08 h / Inert atmosphere
4.2: 80 °C
With
ammonium acetate; sodium carbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; chloroform; water; toluene; butan-1-ol;
4.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/ejoc.201301300
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine / chloroform / 1 h
1.2: 20 °C
2.1: sodium carbonate / water; tetrahydrofuran; toluene / 0.08 h / Inert atmosphere
2.2: 80 °C
With
sodium carbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; chloroform; water; toluene;
2.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/ejoc.201301300
