Technology Process of C52H64N6O12
There total 4 articles about C52H64N6O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C53H66N6O12;
With
lithium hydroxide monohydrate; dihydrogen peroxide;
In
methanol;
at 0 ℃;
for 1h;
In
methanol;
at 20 ℃;
for 22h;
DOI:10.1002/chem.201103185
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / tetrahydrofuran / 48 h / 0 - 20 °C
2.1: lithium hydroxide monohydrate; dihydrogen peroxide / methanol / 1 h / 0 °C
2.2: 22 h / 20 °C
With
lithium hydroxide monohydrate; dihydrogen peroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one;
In
tetrahydrofuran; methanol;
DOI:10.1002/chem.201103185
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / 1 h / 0 °C
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / tetrahydrofuran / 48 h / 0 - 20 °C
3.1: lithium hydroxide monohydrate; dihydrogen peroxide / methanol / 1 h / 0 °C
3.2: 22 h / 20 °C
With
lithium hydroxide monohydrate; dihydrogen peroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; trifluoroacetic acid;
In
tetrahydrofuran; methanol;
DOI:10.1002/chem.201103185
