N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

Base Information

• Chemical Name: N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide
• CAS No.: 452089-45-1
• Molecular Formula: C₂₂H₂₀N₂O₃S
• Molecular Weight: 392.478

Synonyms:N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

Chemical Property of N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

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Technology Process of N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

There total 3 articles about N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N-(4-hydroxy-2,5-dimethylphenyl)-N'-(4-methylphenylsulfonyl)benzimidamide (461672-30-0) → N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide (452089-45-1)

Guidance literature:

With lead(IV) tetraacetate; In acetic acid;

DOI:10.1134/S1070428009030063

Reference yield:

N-(tolylsulfonyl)benzimidoyl chloride (4513-27-3) → N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide (452089-45-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium acetate / acetic acid; N,N-dimethyl-formamide

2: lead(IV) tetraacetate / acetic acid

With sodium acetate; lead(IV) tetraacetate; In acetic acid; N,N-dimethyl-formamide;

DOI:10.1134/S107042801207007X

Reference yield:

2,5-dimethyl-4-amino phenol (3096-71-7) → N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide (452089-45-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium acetate / acetic acid; N,N-dimethyl-formamide

2: lead(IV) tetraacetate / acetic acid

With sodium acetate; lead(IV) tetraacetate; In acetic acid; N,N-dimethyl-formamide;

DOI:10.1134/S107042801207007X

upstream raw materials:

N-(4-hydroxy-2,5-dimethylphenyl)-N'-(4-methylphenylsulfonyl)benzimidamide

N-(tolylsulfonyl)benzimidoyl chloride

2,5-dimethyl-4-amino phenol

Downstream raw materials:

2,5-dimethyl-4-[(4-methylphenylsulfonylimino)(phenyl)methylamino]phenyl 4-methoxybenzenesulfonate

N-[4-hydroxy-3-(4-methoxyphenylsulfonyl)-2,5-dimethylphenyl]-N'-(4-methylphenylsulfonyl)benzimidamide

N-(2,5-dichloro-3,6-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzimidamide

N-(2,5-dibromo-4-hydroxy-3,6-dimethylphenyl)-N'-(4-methylphenylsulfonyl)benzimidamide

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