(3R,4S)-3-(benzyloxycarbonylamino)-4-(methoxymethoxy)nona-1-ene

Base Information

• Chemical Name: (3R,4S)-3-(benzyloxycarbonylamino)-4-(methoxymethoxy)nona-1-ene
• CAS No.: 1253959-12-4
• Molecular Formula: C₁₉H₂₉NO₄
• Molecular Weight: 335.444
• Mol file: 1253959-12-4.mol

Synonyms:(3R,4S)-3-(benzyloxycarbonylamino)-4-(methoxymethoxy)nona-1-ene

Chemical Property of (3R,4S)-3-(benzyloxycarbonylamino)-4-(methoxymethoxy)nona-1-ene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (3R,4S)-3-(benzyloxycarbonylamino)-4-(methoxymethoxy)nona-1-ene

There total 1 articles about (3R,4S)-3-(benzyloxycarbonylamino)-4-(methoxymethoxy)nona-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C11H23NO2 + benzyl chloroformate (501-53-1,94274-21-2) → (3R,4S)-3-(benzyloxycarbonylamino)-4-(methoxymethoxy)nona-1-ene (1253959-12-4)

Guidance literature:

at 20 ℃;

DOI:10.1039/c0ob00219d

Reference yield: 87.0%

2-vinyl-1,3-dioxolane (3984-22-3) + (3R,4S)-3-(benzyloxycarbonylamino)-4-(methoxymethoxy)nona-1-ene (1253959-12-4) → 2-[(1E,3R,4S)-3-(benzyloxycarbonylamino)-4-(methoxymethoxy)nona-2-enyl]-1,3-dioxolane (1253959-15-7)

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; Inert atmosphere; Reflux;

DOI:10.1039/c0ob00219d

upstream raw materials:

benzyl chloroformate

Downstream raw materials:

2-[(1E,3R,4S)-3-(benzyloxycarbonylamino)-4-(methoxymethoxy)nona-2-enyl]-1,3-dioxolane