C₄₀H₆₁NO₈SSi₂

Base Information

Chemical Name:C₄₀H₆₁NO₈SSi₂
CAS No.:1622094-37-4
Molecular Formula:C₄₀H₆₁NO₈SSi₂
Molecular Weight:772.163
Hs Code.:

C<sub>40</sub>H<sub>61</sub>NO<sub>8</sub>SSi<sub>2</sub>

Synonyms:C₄₀H₆₁NO₈SSi₂

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Chemical Property of C₄₀H₆₁NO₈SSi₂

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Technology Process of C₄₀H₆₁NO₈SSi₂

There total 13 articles about C₄₀H₆₁NO₈SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1622094-28-3
C₄₀H₅₉NO₈SSi₂

: 1622094-37-4
C₄₀H₆₁NO₈SSi₂

Guidance literature:: With lithium borohydride; In tetrahydrofuran; at -78 ℃; for 6h; Inert atmosphere;
DOI:10.1002/chem.201402323

Reference yield:

: 179260-96-9
4-methoxy-3-(triisopropylsilyloxy)-benzaldehyde

: 1622094-37-4
C₄₀H₆₁NO₈SSi₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: silver nitrate; iodine / dichloromethane / 14 h / 20 °C / Inert atmosphere

2.1: copper dichloride; tert.-butylhydroperoxide / acetonitrile; water / 16 h / 20 - 50 °C

3.1: thionyl chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere; Reflux

4.1: water; tetrahydrofuran / 0.08 h

4.2: 2 h / 0 °C

5.1: lithium iodide monohydrate / ethyl acetate / 48 h / 20 °C / Reflux

6.1: [bis(acetoxy)iodo]benzene / dichloromethane / 0.17 h / 20 °C

7.1: potassium hydroxide / water; methanol / 0.25 h / -20 °C

8.1: 2,6-dimethylpyridine / dichloromethane / 3 h / 20 °C / Inert atmosphere

9.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

10.1: triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

11.1: lithium borohydride / tetrahydrofuran / 6 h / -78 °C / Inert atmosphere

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; lithium borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; lithium iodide monohydrate; [bis(acetoxy)iodo]benzene; iodine; silver nitrate; triethylamine; potassium hydroxide; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile; 4.1: |Schotten-Baumann Reaction;
DOI:10.1002/chem.201402323

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 1622094-37-4
C₄₀H₆₁NO₈SSi₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

2.1: silver nitrate; iodine / dichloromethane / 14 h / 20 °C / Inert atmosphere

3.1: copper dichloride; tert.-butylhydroperoxide / acetonitrile; water / 16 h / 20 - 50 °C

4.1: thionyl chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere; Reflux

5.1: water; tetrahydrofuran / 0.08 h

5.2: 2 h / 0 °C

6.1: lithium iodide monohydrate / ethyl acetate / 48 h / 20 °C / Reflux

7.1: [bis(acetoxy)iodo]benzene / dichloromethane / 0.17 h / 20 °C

8.1: potassium hydroxide / water; methanol / 0.25 h / -20 °C

9.1: 2,6-dimethylpyridine / dichloromethane / 3 h / 20 °C / Inert atmosphere

10.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

11.1: triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

12.1: lithium borohydride / tetrahydrofuran / 6 h / -78 °C / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; tert.-butylhydroperoxide; lithium borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; lithium iodide monohydrate; [bis(acetoxy)iodo]benzene; iodine; silver nitrate; triethylamine; potassium hydroxide; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 5.1: |Schotten-Baumann Reaction;
DOI:10.1002/chem.201402323