bis[2,4-bis(trifluoromethyl)phenyl]diethylaminophosphane

Base Information

• Chemical Name: bis[2,4-bis(trifluoromethyl)phenyl]diethylaminophosphane
• CAS No.: 1039309-32-4
• Molecular Formula: C₂₀H₁₆F₁₂NP
• Molecular Weight: 529.308
• Mol file: 1039309-32-4.mol

Synonyms:bis[2,4-bis(trifluoromethyl)phenyl]diethylaminophosphane

Chemical Property of bis[2,4-bis(trifluoromethyl)phenyl]diethylaminophosphane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of bis[2,4-bis(trifluoromethyl)phenyl]diethylaminophosphane

There total 1 articles about bis[2,4-bis(trifluoromethyl)phenyl]diethylaminophosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethylphosphoramidous dichloride (1069-08-5) + 1,3-bis(trifluoromethyl)benzene (402-31-3) → bis[2,4-bis(trifluoromethyl)phenyl]diethylaminophosphane (1039309-32-4)

Guidance literature:

1,3-bis(trifluoromethyl)benzene; With n-butyllithium;

With phosphorus trichloride;

diethylphosphoramidous dichloride;

DOI:10.1002/anie.200801025

Reference yield: 84.0%

bis[2,4-bis(trifluoromethyl)phenyl]diethylaminophosphane (1039309-32-4) → bromo-bis-(2,4-bis-(trifluoromethyl)-phenyl)-phosphane

Guidance literature:

With hydrogen bromide; In diethyl ether; at -15 - 20 ℃; for 0.5h;

DOI:10.1002/ejic.201900728

Reference yield:

bis[2,4-bis(trifluoromethyl)phenyl]diethylaminophosphane (1039309-32-4) → chloro-bis-(2,4-bis-(trifluoromethyl)-phenyl)-phosphane (525602-71-5)

Guidance literature:

With hydrogenchloride; In chloroform; water;

DOI:10.1002/anie.200801025

upstream raw materials:

diethylphosphoramidous dichloride

1,3-bis(trifluoromethyl)benzene

Downstream raw materials:

chloro-bis-(2,4-bis-(trifluoromethyl)-phenyl)-phosphane