(R,S)-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-N₅-(phenylmethoxycarbonyl)-ornithine

Base Information

• Chemical Name: (R,S)-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-N₅-(phenylmethoxycarbonyl)-ornithine
• CAS No.: 191871-40-6
• Molecular Formula: C₂₀H₂₁Cl₂N₃O₅
• Molecular Weight: 454.31

Synonyms:(R,S)-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-N₅-(phenylmethoxycarbonyl)-ornithine

Chemical Property of (R,S)-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-N₅-(phenylmethoxycarbonyl)-ornithine

Chemical Property:

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Technology Process of (R,S)-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-N₅-(phenylmethoxycarbonyl)-ornithine

There total 1 articles about (R,S)-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-N₅-(phenylmethoxycarbonyl)-ornithine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3,4-dichlorophenyl)-4-[3-[(phenylmethoxycarbonyl)amino]propyl]-imidazolidin-2,5-dione (191871-39-3) → (R,S)-N2-[[(3,4-dichlorophenyl)amino]carbonyl]-N5-(phenylmethoxycarbonyl)-ornithine (191871-40-6)

Guidance literature:

Reference yield: 87.0%

2-[4-(aminomethyl)phenyl]acetamide (181466-81-9) + (R,S)-N2-[[(3,4-dichlorophenyl)amino]carbonyl]-N5-(phenylmethoxycarbonyl)-ornithine (191871-40-6) → (R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N2-[[(3,4-dichlorophenyl)amino]carbonyl]-N5-(phenylmethoxycarbonyl)-ornithinamide

Guidance literature:

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate;

Reference yield:

(R,S)-N2-[[(3,4-dichlorophenyl)amino]carbonyl]-N5-(phenylmethoxycarbonyl)-ornithine (191871-40-6) → (R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N2-[[(3,4-dichlorophenyl)amino]carbonyl]-N5-(1H-imidazol-2-yl)-ornithinamide

Guidance literature:

Multi-step reaction with 3 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate

2: hydrogen bromide / (2S)-N-methyl-1-phenylpropan-2-amine hydrate; acetic acid; ethyl acetate

3: pyridine

With pyridine; hydrogen bromide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; acetic acid; ethyl acetate;

upstream raw materials:

1-(3,4-dichlorophenyl)-4-[3-[(phenylmethoxycarbonyl)amino]propyl]-imidazolidin-2,5-dione

Downstream raw materials:

(R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-ornithinamide

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