methyl (2R,3R)-3-hydroxy-2-[(4-methylcyclohexyl)methyl]-4-methylpentanoate

Base Information

Chemical Name:methyl (2R,3R)-3-hydroxy-2-[(4-methylcyclohexyl)methyl]-4-methylpentanoate
CAS No.:313255-12-8
Molecular Formula:C₁₅H₂₈O₃
Molecular Weight:256.386
Hs Code.:

Synonyms:methyl (2R,3R)-3-hydroxy-2-[(4-methylcyclohexyl)methyl]-4-methylpentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2R,3R)-3-hydroxy-2-[(4-methylcyclohexyl)methyl]-4-methylpentanoate

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Technology Process of methyl (2R,3R)-3-hydroxy-2-[(4-methylcyclohexyl)methyl]-4-methylpentanoate

There total 2 articles about methyl (2R,3R)-3-hydroxy-2-[(4-methylcyclohexyl)methyl]-4-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 313219-57-7
methyl (2R,3R)-3-hydroxy-4-methyl-2-(4-methylbenzyl)pentanoate

: 313255-12-8
methyl (2R,3R)-3-hydroxy-2-[(4-methylcyclohexyl)methyl]-4-methylpentanoate

Guidance literature:: With hydrogen; Rh/Al₂O₃; In methanol; under 3620.13 Torr;
DOI:10.1021/jm0102654

Reference yield:

: 65596-31-8,76835-65-9,114489-57-5,110097-32-0
methyl (S)-3-hydroxy-4-methylvalerate

: 313255-12-8
methyl (2R,3R)-3-hydroxy-2-[(4-methylcyclohexyl)methyl]-4-methylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: LDA; DMPU / tetrahydrofuran / -78 - 0 °C

2: 70 percent / H₂ / Rh/Al₂O₃ / methanol / 3620.13 Torr

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; hydrogen; lithium diisopropyl amide; Rh/Al₂O₃; In tetrahydrofuran; methanol; 1: Frater-Seebach alkylation;
DOI:10.1021/jm0102654