(2S,2'S)-N,N'-(1,4-phenylenebis(methylene))bis(2-azido-3-phenylpropanamide)

Base Information

Chemical Name:(2S,2'S)-N,N'-(1,4-phenylenebis(methylene))bis(2-azido-3-phenylpropanamide)
CAS No.:1400696-72-1
Molecular Formula:C₂₆H₂₆N₈O₂
Molecular Weight:482.545
Hs Code.:

Synonyms:(2S,2'S)-N,N'-(1,4-phenylenebis(methylene))bis(2-azido-3-phenylpropanamide)

Suppliers and Price of (2S,2'S)-N,N'-(1,4-phenylenebis(methylene))bis(2-azido-3-phenylpropanamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,2'S)-N,N'-(1,4-phenylenebis(methylene))bis(2-azido-3-phenylpropanamide)

Chemical Property:

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Technology Process of (2S,2'S)-N,N'-(1,4-phenylenebis(methylene))bis(2-azido-3-phenylpropanamide)

There total 3 articles about (2S,2'S)-N,N'-(1,4-phenylenebis(methylene))bis(2-azido-3-phenylpropanamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 539-48-0
p-xylylidenediamine

: 189571-36-6
(S)-2-Azido-3-phenyl-propionyl chloride

: 1400696-72-1
(2S,2'S)-N,N'-(1,4-phenylenebis(methylene))bis(2-azido-3-phenylpropanamide)

Guidance literature:: With sodium carbonate; In dichloromethane; water; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c2ob26272j

Reference yield:

: 79410-35-8
(2S)-2-azido-3-phenylpropanoic acid

: 1400696-72-1
(2S,2'S)-N,N'-(1,4-phenylenebis(methylene))bis(2-azido-3-phenylpropanamide)

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: sodium carbonate / dichloromethane; water / 18 h / 20 °C / Inert atmosphere

With sodium carbonate; N,N-dimethyl-formamide; In dichloromethane; water;
DOI:10.1039/c2ob26272j

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 1400696-72-1
(2S,2'S)-N,N'-(1,4-phenylenebis(methylene))bis(2-azido-3-phenylpropanamide)

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole-1-sulfonyl azide hydrochloride; potassium carbonate; copper(ll) sulfate pentahydrate / methanol / 18 h / 20 °C

2: N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: sodium carbonate / dichloromethane; water / 18 h / 20 °C / Inert atmosphere

With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; sodium carbonate; potassium carbonate; N,N-dimethyl-formamide; In methanol; dichloromethane; water;
DOI:10.1039/c2ob26272j