octanoic acid 2-[12-(9-diethylamino-5-oxo-5H-benzo[a]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9H-fluoren-9-ylmethoxy)-phosphoryloxymethyl]-ethyl ester

Base Information

Chemical Name:octanoic acid 2-[12-(9-diethylamino-5-oxo-5H-benzo[a]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9H-fluoren-9-ylmethoxy)-phosphoryloxymethyl]-ethyl ester
CAS No.:603136-84-1
Molecular Formula:C₆₆H₈₂N₃O₁₄P
Molecular Weight:1172.36
Hs Code.:

octanoic acid 2-[12-(9-diethylamino-5-oxo-5<i>H</i>-benzo[<i>a</i>]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9<i>H</i>-fluoren-9-ylmethoxy)-phosphoryloxymethyl]-ethyl ester

Synonyms:octanoic acid 2-[12-(9-diethylamino-5-oxo-5H-benzo[a]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9H-fluoren-9-ylmethoxy)-phosphoryloxymethyl]-ethyl ester

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Chemical Property of octanoic acid 2-[12-(9-diethylamino-5-oxo-5H-benzo[a]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9H-fluoren-9-ylmethoxy)-phosphoryloxymethyl]-ethyl ester

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Technology Process of octanoic acid 2-[12-(9-diethylamino-5-oxo-5H-benzo[a]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9H-fluoren-9-ylmethoxy)-phosphoryloxymethyl]-ethyl ester

There total 4 articles about octanoic acid 2-[12-(9-diethylamino-5-oxo-5H-benzo[a]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9H-fluoren-9-ylmethoxy)-phosphoryloxymethyl]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: octanoic acid 2-[12-(9-diethylamino-5-oxo-5H-benzo[a]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9H-fluoren-9-ylmethoxy)-phosphanyloxymethyl]-ethyl ester

: 603136-84-1
octanoic acid 2-[12-(9-diethylamino-5-oxo-5H-benzo[a]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9H-fluoren-9-ylmethoxy)-phosphoryloxymethyl]-ethyl ester

Guidance literature:: With tert.-butylhydroperoxide; at 20 ℃;
DOI:10.1016/S0040-4039(02)02832-0

Reference yield:

: 1016-58-6
6-nitroveratryl alcohol

: 603136-84-1
octanoic acid 2-[12-(9-diethylamino-5-oxo-5H-benzo[a]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9H-fluoren-9-ylmethoxy)-phosphoryloxymethyl]-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diisopropylamine tetrazolide / CH₂Cl₂ / 16 h / 0 - 20 °C

2: tetrazole / 5 h

3: t-BuOOH / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; N,N-diisopropylamine tetrazolide; In dichloromethane;
DOI:10.1016/S0040-4039(02)02832-0

Reference yield:

: 603136-74-9
9H-fluorene-9-ylmethyl N,N,N’,N’-tetraisopropylphosphoramidite

: 603136-84-1
octanoic acid 2-[12-(9-diethylamino-5-oxo-5H-benzo[a]phenoxazin-2-yloxy)-dodecyloxy]-1-[(4,5-dimethoxy-2-nitro-benzyloxy)-(9H-fluoren-9-ylmethoxy)-phosphoryloxymethyl]-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diisopropylamine tetrazolide / CH₂Cl₂ / 16 h / 0 - 20 °C

2: tetrazole / 5 h

3: t-BuOOH / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; N,N-diisopropylamine tetrazolide; In dichloromethane;
DOI:10.1016/S0040-4039(02)02832-0