(1R,2R,4R,5R)-bis((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4,5-bis(benzyloxy)cyclohexane-1,2-dicarboxylate

Base Information

Chemical Name:(1R,2R,4R,5R)-bis((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4,5-bis(benzyloxy)cyclohexane-1,2-dicarboxylate
CAS No.:956006-03-4
Molecular Formula:C₄₂H₆₀O₆
Molecular Weight:660.935
Hs Code.:

Synonyms:(1R,2R,4R,5R)-bis((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4,5-bis(benzyloxy)cyclohexane-1,2-dicarboxylate

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Chemical Property of (1R,2R,4R,5R)-bis((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4,5-bis(benzyloxy)cyclohexane-1,2-dicarboxylate

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Technology Process of (1R,2R,4R,5R)-bis((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4,5-bis(benzyloxy)cyclohexane-1,2-dicarboxylate

There total 3 articles about (1R,2R,4R,5R)-bis((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4,5-bis(benzyloxy)cyclohexane-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 956006-35-2
(1R,2R,4R,5R)-bis((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4-(benzyloxy)-5-hydroxycyclohexane-1,2-dicarboxylate

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 956006-03-4
(1R,2R,4R,5R)-bis((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4,5-bis(benzyloxy)cyclohexane-1,2-dicarboxylate

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; cyclohexane; at 20 ℃; for 24h;
DOI:10.1021/ol7017938

Reference yield:

: 73627-88-0,109062-95-5,110416-37-0,122044-47-7
(1R,2R,1'S,2'R,5'S)-cyclohex-4-ene-1,2-dicarboxylic acid bis(2'-isopropyl-5'-methyl-cyclohexyl) ester

: 956006-03-4
(1R,2R,4R,5R)-bis((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4,5-bis(benzyloxy)cyclohexane-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / mCPBA / CH₂Cl₂ / 3 h

2: 89 percent / Cu(OTf)2 / 24 h

3: 99 percent / TfOH / CH₂Cl₂; cyclohexane / 24 h / 20 °C

With trifluorormethanesulfonic acid; copper(II) bis(trifluoromethanesulfonate); 3-chloro-benzenecarboperoxoic acid; In dichloromethane; cyclohexane;
DOI:10.1021/ol7017938

Reference yield:

: 956006-34-1
(1S,3R,4R,6R)-3-((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4-((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 7-oxabicyclo[4.1.0]heptane-3,4-dicarboxylate

: 956006-03-4
(1R,2R,4R,5R)-bis((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl) 4,5-bis(benzyloxy)cyclohexane-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Cu(OTf)2 / 24 h

2: 99 percent / TfOH / CH₂Cl₂; cyclohexane / 24 h / 20 °C

With trifluorormethanesulfonic acid; copper(II) bis(trifluoromethanesulfonate); In dichloromethane; cyclohexane;
DOI:10.1021/ol7017938