Phenyl-[4-phenyl-6-((E)-styryl)-3-(triphenyl-λ⁵-phosphanylidene)-3,4-dihydro-pyran-(2Z)-ylidene]-amine

Base Information

• Chemical Name: Phenyl-[4-phenyl-6-((E)-styryl)-3-(triphenyl-λ⁵-phosphanylidene)-3,4-dihydro-pyran-(2Z)-ylidene]-amine
• CAS No.: 90963-67-0
• Molecular Formula: C₄₃H₃₄NOP
• Molecular Weight: 611.723

Synonyms:Phenyl-[4-phenyl-6-((E)-styryl)-3-(triphenyl-λ⁵-phosphanylidene)-3,4-dihydro-pyran-(2Z)-ylidene]-amine

Chemical Property of Phenyl-[4-phenyl-6-((E)-styryl)-3-(triphenyl-λ⁵-phosphanylidene)-3,4-dihydro-pyran-(2Z)-ylidene]-amine

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Technology Process of Phenyl-[4-phenyl-6-((E)-styryl)-3-(triphenyl-λ⁵-phosphanylidene)-3,4-dihydro-pyran-(2Z)-ylidene]-amine

There total 1 articles about Phenyl-[4-phenyl-6-((E)-styryl)-3-(triphenyl-λ⁵-phosphanylidene)-3,4-dihydro-pyran-(2Z)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

(N-phenyliminovinylidene)triphenylphosphorane (64448-06-2,21385-80-8) + 1,5-diphenyl-1,4-pentadiene-3-one (538-58-9) → Phenyl-[4-phenyl-6-((E)-styryl)-3-(triphenyl-λ5-phosphanylidene)-3,4-dihydro-pyran-(2Z)-ylidene]-amine (90963-67-0)

Guidance literature:

In tetrahydrofuran; for 4h; Heating;

DOI:10.1016/S0040-4039(01)80181-7

Reference yield: 55.0%

Phenyl-[4-phenyl-6-((E)-styryl)-3-(triphenyl-λ5-phosphanylidene)-3,4-dihydro-pyran-(2Z)-ylidene]-amine (90963-67-0) → (E)-5-Oxo-3,7,N-triphenyl-hept-6-enimidic acid methyl ester (90963-91-0) + Triphenylphosphine oxide (791-28-6)

Guidance literature:

With water; In methanol; Heating;

DOI:10.1016/S0040-4039(01)80181-7

Reference yield: 44.0%

Phenyl-[4-phenyl-6-((E)-styryl)-3-(triphenyl-λ5-phosphanylidene)-3,4-dihydro-pyran-(2Z)-ylidene]-amine (90963-67-0) → Phenyl-[4-phenyl-6-((E)-styryl)-pyran-(2Z)-ylidene]-amine (90963-82-9) + triphenylphosphine (603-35-0)

Guidance literature:

With benzoic acid; Heating;

DOI:10.1016/S0040-4039(01)80181-7

upstream raw materials:

(N-phenyliminovinylidene)triphenylphosphorane

1,5-diphenyl-1,4-pentadiene-3-one

Downstream raw materials:

Phenyl-[4-phenyl-6-((E)-styryl)-pyran-(2Z)-ylidene]-amine

triphenylphosphine

(E)-5-Oxo-3,7,N-triphenyl-hept-6-enimidic acid methyl ester

Triphenylphosphine oxide

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