7-(tert-butyldimethylsilyloxy)-1-diphenylphosphinyl-1-methoxy-2-heptanone

Base Information

Chemical Name:7-(tert-butyldimethylsilyloxy)-1-diphenylphosphinyl-1-methoxy-2-heptanone
CAS No.:365414-49-9
Molecular Formula:C₂₆H₃₉O₄PSi
Molecular Weight:474.653
Hs Code.:

Synonyms:7-(tert-butyldimethylsilyloxy)-1-diphenylphosphinyl-1-methoxy-2-heptanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(tert-butyldimethylsilyloxy)-1-diphenylphosphinyl-1-methoxy-2-heptanone

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Technology Process of 7-(tert-butyldimethylsilyloxy)-1-diphenylphosphinyl-1-methoxy-2-heptanone

There total 1 articles about 7-(tert-butyldimethylsilyloxy)-1-diphenylphosphinyl-1-methoxy-2-heptanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 4455-77-0
(methoxymethyl)diphenylphosphine oxide

: 161232-10-6
6-(tert-butyl-dimethylsilanoxy)hexanoic acid methyl ester

: 365414-49-9
7-(tert-butyldimethylsilyloxy)-1-diphenylphosphinyl-1-methoxy-2-heptanone

Guidance literature:: (methoxymethyl)diphenylphosphine oxide; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.166667h;

6-(tert-butyl-dimethylsilanoxy)hexanoic acid methyl ester; In tetrahydrofuran; at -78 ℃; for 0.666667h;
DOI:10.1021/jo034853w

Reference yield: 91.0%

: 365414-49-9
7-(tert-butyldimethylsilyloxy)-1-diphenylphosphinyl-1-methoxy-2-heptanone

: 1730-25-2
allylmagnesium bromide

: 7-(tert-butyldimethylsilyloxy)-1-(diphenylphosphinyl)-1-methoxy-2-(2-propenyl)-2-heptanol

Guidance literature:: allylmagnesium bromide; With cerium(III) chloride; In tetrahydrofuran; diethyl ether; for 1h;

7-(tert-butyldimethylsilyloxy)-1-diphenylphosphinyl-1-methoxy-2-heptanone; In tetrahydrofuran; diethyl ether; at 0 ℃; for 1h;
DOI:10.1021/jo034853w