4,4'-bis[1,3-di(tert-butoxycarbonyl)-2-imidazolidinylimino]diphenylamine

Base Information

Chemical Name:4,4'-bis[1,3-di(tert-butoxycarbonyl)-2-imidazolidinylimino]diphenylamine
CAS No.:292634-05-0
Molecular Formula:C₃₈H₅₃N₇O₈
Molecular Weight:735.881
Hs Code.:

Synonyms:4,4'-bis[1,3-di(tert-butoxycarbonyl)-2-imidazolidinylimino]diphenylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-bis[1,3-di(tert-butoxycarbonyl)-2-imidazolidinylimino]diphenylamine

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Technology Process of 4,4'-bis[1,3-di(tert-butoxycarbonyl)-2-imidazolidinylimino]diphenylamine

There total 2 articles about 4,4'-bis[1,3-di(tert-butoxycarbonyl)-2-imidazolidinylimino]diphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 537-65-5
4,4'-diaminodiphenylamine

: 173300-83-9
2-thioxo-imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester

: 292634-05-0
4,4'-bis[1,3-di(tert-butoxycarbonyl)-2-imidazolidinylimino]diphenylamine

Guidance literature:: With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/S0968-0896(00)00089-4

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 292634-05-0
4,4'-bis[1,3-di(tert-butoxycarbonyl)-2-imidazolidinylimino]diphenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / NaH / tetrahydrofuran / 4 h / 20 °C

2: 76 percent / Et₃N; HgCl₂ / dimethylformamide / 0 - 20 °C

With sodium hydride; triethylamine; mercury dichloride; In tetrahydrofuran; N,N-dimethyl-formamide; 1: Acylation / 2: Substitution;
DOI:10.1016/S0968-0896(00)00089-4