C₁₈H₁₇FN₆O

Base Information

Chemical Name:C₁₈H₁₇FN₆O
CAS No.:1609528-73-5
Molecular Formula:C₁₈H₁₇FN₆O
Molecular Weight:352.371
Hs Code.:

C<sub>18</sub>H<sub>17</sub>FN<sub>6</sub>O

Synonyms:C₁₈H₁₇FN₆O

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Chemical Property of C₁₈H₁₇FN₆O

Chemical Property:

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Technology Process of C₁₈H₁₇FN₆O

There total 4 articles about C₁₈H₁₇FN₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609531-00-1
C₁₂H₁₀FN₃O₃

: 1609528-73-5
C₁₈H₁₇FN₆O

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen bromide; acetic acid / 4 h / 110 °C / Sealed tube

2.1: trichlorophosphate; triethylamine / 2 h / 110 °C / Sealed tube

2.2: 1 h / 0 °C

3.1: butan-1-ol / 3 h / 120 °C / Microwave irradiation

With hydrogen bromide; acetic acid; triethylamine; trichlorophosphate; In butan-1-ol;

Reference yield:

: 73027-79-9
4,6-dichloro-nicotinic acid

: 1609528-73-5
C₁₈H₁₇FN₆O

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hydroxide monohydrate / tetrahydrofuran / 1 h / 20 - 25 °C

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; caesium carbonate / N,N-dimethyl acetamide / 0.5 h / 145 °C / Inert atmosphere

3.1: hydrogen bromide; acetic acid / 4 h / 110 °C / Sealed tube

4.1: trichlorophosphate; triethylamine / 2 h / 110 °C / Sealed tube

4.2: 1 h / 0 °C

5.1: butan-1-ol / 3 h / 120 °C / Microwave irradiation

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium hydroxide monohydrate; hydrogen bromide; caesium carbonate; acetic acid; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trichlorophosphate; In tetrahydrofuran; N,N-dimethyl acetamide; butan-1-ol;

Reference yield:

: 1609531-01-2
C₁₁H₈FN₃O₃

: 1609528-73-5
C₁₈H₁₇FN₆O

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate; triethylamine / 2 h / 110 °C / Sealed tube

1.2: 1 h / 0 °C

2.1: butan-1-ol / 3 h / 120 °C / Microwave irradiation

With triethylamine; trichlorophosphate; In butan-1-ol;