2-(diphenylphosphonooxy)ethyl 2-deoxy-2-(N-dodecanoylglycylamino)-4,6-O-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

Base Information

Chemical Name:2-(diphenylphosphonooxy)ethyl 2-deoxy-2-(N-dodecanoylglycylamino)-4,6-O-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside
CAS No.:123573-86-4
Molecular Formula:C₅₁H₈₁N₂O₁₂P
Molecular Weight:945.184
Hs Code.:

Synonyms:2-(diphenylphosphonooxy)ethyl 2-deoxy-2-(N-dodecanoylglycylamino)-4,6-O-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

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Chemical Property of 2-(diphenylphosphonooxy)ethyl 2-deoxy-2-(N-dodecanoylglycylamino)-4,6-O-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

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Technology Process of 2-(diphenylphosphonooxy)ethyl 2-deoxy-2-(N-dodecanoylglycylamino)-4,6-O-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

There total 6 articles about 2-(diphenylphosphonooxy)ethyl 2-deoxy-2-(N-dodecanoylglycylamino)-4,6-O-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112-16-3
n-dodecanoyl chloride

: 123573-86-4
2-(diphenylphosphonooxy)ethyl 2-deoxy-2-(N-dodecanoylglycylamino)-4,6-O-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / aq. NaOH / 0.5 h

2: DCC / CH₂Cl₂ / 1 h / Ambient temperature

With sodium hydroxide; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1248/cpb.39.3244

Reference yield:

: 123573-82-0
2-hydroxyethyl 2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 123573-86-4
2-(diphenylphosphonooxy)ethyl 2-deoxy-2-(N-dodecanoylglycylamino)-4,6-O-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / p-TsOH*H₂O / dimethylformamide / 3.5 h

2: 71.8 percent / pyridine, DMAP / CH₂Cl₂; methanol / 4 h

3: 74 percent / pyridine, DMAP / CH₂Cl₂

4: Zn, AcOH / 1 h / Ambient temperature

5: DCC / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; dmap; toluene-4-sulfonic acid; acetic acid; dicyclohexyl-carbodiimide; zinc; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.3244

Reference yield:

: 123573-83-1
2-hydroxyethyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 123573-86-4
2-(diphenylphosphonooxy)ethyl 2-deoxy-2-(N-dodecanoylglycylamino)-4,6-O-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 71.8 percent / pyridine, DMAP / CH₂Cl₂; methanol / 4 h

2: 74 percent / pyridine, DMAP / CH₂Cl₂

3: Zn, AcOH / 1 h / Ambient temperature

4: DCC / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; dmap; acetic acid; dicyclohexyl-carbodiimide; zinc; In methanol; dichloromethane;
DOI:10.1248/cpb.39.3244