benzoyl-[1-[(E)-benzylideneamino]-3-butylbenzimidazol-3-ium-2-carbothioyl]azanide

Base Information

Chemical Name:benzoyl-[1-[(E)-benzylideneamino]-3-butylbenzimidazol-3-ium-2-carbothioyl]azanide
CAS No.:1289375-02-5
Molecular Formula:C₂₆H₂₄N₄OS
Molecular Weight:440.569
Hs Code.:

Synonyms:benzoyl-[1-[(E)-benzylideneamino]-3-butylbenzimidazol-3-ium-2-carbothioyl]azanide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoyl-[1-[(E)-benzylideneamino]-3-butylbenzimidazol-3-ium-2-carbothioyl]azanide

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Technology Process of benzoyl-[1-[(E)-benzylideneamino]-3-butylbenzimidazol-3-ium-2-carbothioyl]azanide

There total 4 articles about benzoyl-[1-[(E)-benzylideneamino]-3-butylbenzimidazol-3-ium-2-carbothioyl]azanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: (E)-N-(3-butylbenzimidazol-3-ium-1-yl)-1-phenylmethanimine iodide

: 532-55-8
Benzoyl isothiocyanate

: 1289375-02-5
benzoyl-[1-[(E)-benzylideneamino]-3-butylbenzimidazol-3-ium-2-carbothioyl]azanide

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jo200088s

Reference yield:

: 6299-92-9
1-aminobenzimidazole

: 1289375-02-5
benzoyl-[1-[(E)-benzylideneamino]-3-butylbenzimidazol-3-ium-2-carbothioyl]azanide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / ethanol / 5 h

2: 5 h / 100 °C

3: sodium hydride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

With sulfuric acid; sodium hydride; In tetrahydrofuran; ethanol;
DOI:10.1021/jo200088s

Reference yield:

: 81949-11-3
(E)-N-(benzimidazol-1-yl)-1-phenyl-methanimine

: 1289375-02-5
benzoyl-[1-[(E)-benzylideneamino]-3-butylbenzimidazol-3-ium-2-carbothioyl]azanide

Guidance literature:: Multi-step reaction with 2 steps

1: 5 h / 100 °C

2: sodium hydride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo200088s