C₄₆H₆₈N₄O₆Si

Base Information

• Chemical Name: C₄₆H₆₈N₄O₆Si
• CAS No.: 1070774-57-0
• Molecular Formula: C₄₆H₆₈N₄O₆Si
• Molecular Weight: 801.155
• Mol file: 1070774-57-0.mol

Synonyms:C₄₆H₆₈N₄O₆Si

Chemical Property of C₄₆H₆₈N₄O₆Si

Chemical Property:

Purity/Quality:

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Technology Process of C₄₆H₆₈N₄O₆Si

There total 1 articles about C₄₆H₆₈N₄O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

erythro-(-)-3-methyl-4-penten-2-ol (99438-31-0) + Pea-Ala-D-N-MeTrp-β-Tyr(TIPS)-OH (1070774-48-9) → C46H68N4O6Si (1070774-57-0)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 23 ℃; Inert atmosphere;

DOI:10.1021/ja9095126

Reference yield: 48.0%

C46H68N4O6Si (1070774-57-0) → C44H64N4O6Si (1070774-62-7)

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 110 ℃; for 2h; stereoselective reaction; Inert atmosphere;

DOI:10.1002/anie.200801010

upstream raw materials:

erythro-(-)-3-methyl-4-penten-2-ol

Pea-Ala-D-N-MeTrp-β-Tyr(TIPS)-OH

Downstream raw materials:

C₄₄H₆₄N₄O₆Si