Technology Process of C28H28N2O6S
There total 5 articles about C28H28N2O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 24h;
DOI:10.1016/j.ejmech.2012.08.021
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / dichloromethane / 14 h / 0 - 20 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 5 - 10 °C
3: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C
4: lithium hydroxide monohydrate / tetrahydrofuran; water / 12 h / 20 °C
5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 24 h / 20 °C
With
lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.08.021
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 5 - 10 °C
2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C
3: lithium hydroxide monohydrate / tetrahydrofuran; water / 12 h / 20 °C
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 24 h / 20 °C
With
lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.08.021