7-hydroxy-5-methoxy-2-(2-methoxyphenyl)-4-oxo-4H-chromene-6-carbaldehyde

Base Information

Chemical Name:7-hydroxy-5-methoxy-2-(2-methoxyphenyl)-4-oxo-4H-chromene-6-carbaldehyde
CAS No.:1616883-75-0
Molecular Formula:C₁₈H₁₄O₆
Molecular Weight:326.306
Hs Code.:

Synonyms:7-hydroxy-5-methoxy-2-(2-methoxyphenyl)-4-oxo-4H-chromene-6-carbaldehyde

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Chemical Property of 7-hydroxy-5-methoxy-2-(2-methoxyphenyl)-4-oxo-4H-chromene-6-carbaldehyde

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Technology Process of 7-hydroxy-5-methoxy-2-(2-methoxyphenyl)-4-oxo-4H-chromene-6-carbaldehyde

There total 5 articles about 7-hydroxy-5-methoxy-2-(2-methoxyphenyl)-4-oxo-4H-chromene-6-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1616883-59-0
4-methoxy-7-(2-methoxyphenyl)-5H-furo[3,2-g]chromen-5-one

: 1616883-75-0
7-hydroxy-5-methoxy-2-(2-methoxyphenyl)-4-oxo-4H-chromene-6-carbaldehyde

Guidance literature:: With potassium dichromate; sulfuric acid; acetic acid; at 50 ℃;
DOI:10.1016/j.ejmech.2014.06.007

Reference yield:

: 484-27-5
5-acetyl-4-methoxybenzofuran-6-ol

: 1616883-75-0
7-hydroxy-5-methoxy-2-(2-methoxyphenyl)-4-oxo-4H-chromene-6-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 24 h / 20 °C

2: selenium(IV) oxide / butan-1-ol / 24 h / Reflux

3: acetic acid; sulfuric acid; potassium dichromate / 50 °C

With potassium dichromate; selenium(IV) oxide; sulfuric acid; acetic acid; sodium hydroxide; In ethanol; butan-1-ol; 1: |Claisen-Schmidt Condensation;
DOI:10.1016/j.ejmech.2014.06.007

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 1616883-75-0
7-hydroxy-5-methoxy-2-(2-methoxyphenyl)-4-oxo-4H-chromene-6-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 24 h / 20 °C

2: selenium(IV) oxide / butan-1-ol / 24 h / Reflux

3: acetic acid; sulfuric acid; potassium dichromate / 50 °C

With potassium dichromate; selenium(IV) oxide; sulfuric acid; acetic acid; sodium hydroxide; In ethanol; butan-1-ol; 1: |Claisen-Schmidt Condensation;
DOI:10.1016/j.ejmech.2014.06.007