(1-methylcyclopropyl)methyl tosylate

Base Information

• Chemical Name: (1-methylcyclopropyl)methyl tosylate
• CAS No.: 13033-53-9
• Molecular Formula: C₁₂H₁₆O₃S
• Molecular Weight: 240.323
• Mol file: 13033-53-9.mol

Synonyms:(1-methylcyclopropyl)methyl tosylate

Chemical Property of (1-methylcyclopropyl)methyl tosylate

Chemical Property:

Purity/Quality:

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Technology Process of (1-methylcyclopropyl)methyl tosylate

There total 2 articles about (1-methylcyclopropyl)methyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 1-methylcyclopropanecarboxylate (6206-25-3) → (1-methylcyclopropyl)methyl tosylate (13033-53-9)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄

2: collidine

With 2,3,5-trimethyl-pyridine; lithium aluminium tetrahydride;

DOI:10.1021/jo01344a524

Reference yield:

1-methylcyclopropanemethanol (2746-14-7) + p-toluenesulfonyl chloride (98-59-9) → (1-methylcyclopropyl)methyl tosylate (13033-53-9)

Guidance literature:

With 2,3,5-trimethyl-pyridine;

DOI:10.1021/jo01344a524

upstream raw materials:

1-methylcyclopropanemethanol

p-toluenesulfonyl chloride

methyl 1-methylcyclopropanecarboxylate