C₂₅H₂₆N₄O₁₀S

Base Information

• Chemical Name: C₂₅H₂₆N₄O₁₀S
• CAS No.: 129254-38-2
• Molecular Formula: C₂₅H₂₆N₄O₁₀S
• Molecular Weight: 574.568
• Mol file: 129254-38-2.mol

Synonyms:C₂₅H₂₆N₄O₁₀S

Chemical Property of C₂₅H₂₆N₄O₁₀S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂₅H₂₆N₄O₁₀S

There total 2 articles about C₂₅H₂₆N₄O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

6-Demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-methylidenemitosane (122644-75-1) + para-nitrobenzenethiol (1849-36-1) → C25H26N4O10S (129254-38-2)

Guidance literature:

With triethylamine; In dichloromethane; for 1.5h; Ambient temperature;

DOI:10.1021/jm00038a008

Reference yield:

1a-acetyl-7-demethoxy-6,7-dihydro-7,7-(ethylenedioxy)-6-(phenylselenyl)mitomycin A (122644-74-0,122675-60-9,134679-23-5) → C25H26N4O10S (129254-38-2)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine, mCPBA / CHCl₃ / 0.17 h / Ambient temperature

2: 54 percent / Et₃N / CH₂Cl₂ / 1.5 h / Ambient temperature

With pyridine; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform;

DOI:10.1021/jm00038a008

Reference yield: 4.0%

C25H26N4O10S (129254-38-2) → C21H21N5O7S

Guidance literature:

With ammonia; In tetrahydrofuran; for 168h; Ambient temperature;

DOI:10.1021/jm00038a008

upstream raw materials:

6-Demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-methylidenemitosane

para-nitrobenzenethiol

1a-acetyl-7-demethoxy-6,7-dihydro-7,7-(ethylenedioxy)-6-(phenylselenyl)mitomycin A

Refernces