N-(benzyloxycarbonyl)<α-2H>aminoadipic acid anhydride

Base Information

Chemical Name:N-(benzyloxycarbonyl)<α-2H>aminoadipic acid anhydride
CAS No.:110850-84-5
Molecular Formula:C₁₄H₁₅NO₅
Molecular Weight:278.269
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)<α-2H>aminoadipic acid anhydride

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Chemical Property of N-(benzyloxycarbonyl)<α-2H>aminoadipic acid anhydride

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Technology Process of N-(benzyloxycarbonyl)<α-2H>aminoadipic acid anhydride

There total 6 articles about N-(benzyloxycarbonyl)<α-2H>aminoadipic acid anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 110850-83-4
N-(benzyloxycarbonyl)<α-2H>aminoadipic acid

: 110850-84-5
N-(benzyloxycarbonyl)<α-2H>aminoadipic acid anhydride

Guidance literature:: With acetic anhydride; at 50 ℃; for 1h;
DOI:10.1021/jo00233a007

Reference yield:

: 542-32-5
(R,S)-2-aminoadipic acid

: 110850-84-5
N-(benzyloxycarbonyl)<α-2H>aminoadipic acid anhydride

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / sodium carbonate monohydrate / H₂O / 24 h / Ambient temperature

2: D₂O, Na₂CO₃, acetic anhydride / 48 h / 50 °C

3: 70 percent / 2 N NH₄OH / H₂O / 20 h / 37 °C / porcine kidney acylase

4: 75 percent / sodium bicarbonate / H₂O / 1.) 0 deg C, 4 h, 2.) RT, 8 h

5: 100 percent / acetic anhydride / 1 h / 50 °C

With ammonium hydroxide; water-d2; acetic anhydride; sodium hydrogencarbonate; sodium carbonate; In water;
DOI:10.1021/jo00233a007

Reference yield:

: 110850-82-3
L-<α-2H>aminoadipic acid

: 110850-84-5
N-(benzyloxycarbonyl)<α-2H>aminoadipic acid anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / sodium bicarbonate / H₂O / 1.) 0 deg C, 4 h, 2.) RT, 8 h

2: 100 percent / acetic anhydride / 1 h / 50 °C

With acetic anhydride; sodium hydrogencarbonate; In water;
DOI:10.1021/jo00233a007