N-(4-AMINOBENZYL)-N-METHYL-P-TOLUENESULFONAMIDE

Base Information

• Chemical Name: N-(4-AMINOBENZYL)-N-METHYL-P-TOLUENESULFONAMIDE
• CAS No.: 115562-53-3
• Molecular Formula: C15H18N2O2S
• Molecular Weight: 290.38
• Mol file: 115562-53-3.mol

Synonyms:N-(4-AMINOBENZYL)-N-METHYL-P-TOLUENESULFONAMIDE;N-(4-Aminobenzyl)-N,4-dimethylbenzenesulfonamide

Chemical Property of N-(4-AMINOBENZYL)-N-METHYL-P-TOLUENESULFONAMIDE

Chemical Property:

• Vapor Pressure: 3.29E-09mmHg at 25°C
• Refractive Index: 1.614
• Boiling Point: 475.531 °C at 760 mmHg
• PKA: 4.36±0.10(Predicted)
• Flash Point: 241.393 °C
• PSA: 71.78000
• Density: 1.24 g/cm³
• LogP: 4.05990

Purity/Quality:

99% ^*data from raw suppliers

N-(4-Aminobenzyl)-N-methyl-p-toluenesulfonamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(4-AMINOBENZYL)-N-METHYL-P-TOLUENESULFONAMIDE

There total 3 articles about N-(4-AMINOBENZYL)-N-METHYL-P-TOLUENESULFONAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

N-methyl-N-(4'-nitrobenzyl)-4-toluenesulfonamide (115562-51-1) → N-methyl-N-(4'-aminobenzyl)-4-toluenesulfonamide (115562-53-3)

Guidance literature:

With hydrogenchloride; tin; In ethanol; Heating;

DOI:10.1021/jo00255a005

Reference yield:

1-bromomethyl-4-nitro-benzene (100-11-8) → N-methyl-N-(4'-aminobenzyl)-4-toluenesulfonamide (115562-53-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / KOH / aq. ethanol

2: 76 percent / Sn, HCl, / aq. ethanol / Heating

With hydrogenchloride; potassium hydroxide; tin; In ethanol;

DOI:10.1021/jo00255a005

Reference yield:

N-methyl-p-toluenesulfonylamide (640-61-9) → N-methyl-N-(4'-aminobenzyl)-4-toluenesulfonamide (115562-53-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / KOH / aq. ethanol

2: 76 percent / Sn, HCl, / aq. ethanol / Heating

With hydrogenchloride; potassium hydroxide; tin; In ethanol;

DOI:10.1021/jo00255a005

upstream raw materials:

N-methyl-N-(4'-nitrobenzyl)-4-toluenesulfonamide

1-bromomethyl-4-nitro-benzene

N-methyl-p-toluenesulfonylamide

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