6-(benzyloxycarbonylamino)hexyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Base Information

Chemical Name:6-(benzyloxycarbonylamino)hexyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside
CAS No.:66888-24-2
Molecular Formula:C₂₈H₃₉NO₁₂
Molecular Weight:581.617
Hs Code.:

Synonyms:6-(benzyloxycarbonylamino)hexyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

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Chemical Property of 6-(benzyloxycarbonylamino)hexyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

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Technology Process of 6-(benzyloxycarbonylamino)hexyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

There total 2 articles about 6-(benzyloxycarbonylamino)hexyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 4163-65-9
per-O-acetyl-α-D-mannopyranose

: 66888-24-2
6-(benzyloxycarbonylamino)hexyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: With tin(IV) chloride; In dichloromethane; for 10h; Ambient temperature;
DOI:10.1016/0008-6215(90)84295-6

Reference yield:

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 121238-27-5
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl trichloroimidate

: 66888-24-2
6-(benzyloxycarbonylamino)hexyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; Molecular sieve;
DOI:10.1016/j.carres.2020.107928

Reference yield:

: 66888-24-2
6-(benzyloxycarbonylamino)hexyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 129460-89-5
6-aminohexyl 6-O-(diphenoxyphosphinyl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: CH₃ONa / acetic acid / 1 h / Ambient temperature

2: pyridine / 0.25 h / 0 °C

3: H₂ / 10percent Pd-C / aq. ethanol; aq. acetic acid / Ambient temperature

With pyridine; hydrogen; sodium methylate; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1016/0008-6215(90)84295-6