2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 2,4-dinitrobenzenesulfonate

Base Information

Chemical Name:2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 2,4-dinitrobenzenesulfonate
CAS No.:1345985-98-9
Molecular Formula:C₂₆H₂₇N₃O₉S
Molecular Weight:557.581
Hs Code.:

Synonyms:2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 2,4-dinitrobenzenesulfonate

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Chemical Property of 2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 2,4-dinitrobenzenesulfonate

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Technology Process of 2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 2,4-dinitrobenzenesulfonate

There total 8 articles about 2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 2,4-dinitrobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1656-44-6
2,4-dinitrobenzenesulfonyl chloride

: 215391-96-1
rac-2-(N-tert-Butoxycarbonyl-N-benzylamino)-1-phenylethanol

: 1345985-98-9
2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 2,4-dinitrobenzenesulfonate

Guidance literature:: rac-2-(N-tert-Butoxycarbonyl-N-benzylamino)-1-phenylethanol; With potassium hydroxide; In tetrahydrofuran; for 0.25h;

2,4-dinitrobenzenesulfonyl chloride; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

: 96-09-3
styrene oxide

: 1345985-98-9
2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 2,4-dinitrobenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: activated silica / 24 h / Inert atmosphere

2: triethylamine / methanol / 0.5 h / Reflux

3: potassium hydroxide / tetrahydrofuran / 0.25 h

With triethylamine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

: 51096-49-2,91579-12-3,107171-75-5,27159-30-4
2-benzylamino-1-phenyl-ethanol

: 1345985-98-9
2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 2,4-dinitrobenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol / 0.5 h / Reflux

2: potassium hydroxide / tetrahydrofuran / 0.25 h

With triethylamine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.08.078