Technology Process of C30H27NO7S
There total 8 articles about C30H27NO7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: cesium carbonate, 18-crown-6 / acetonitrile / 40 h / 25 °C
2: acetonitrile; benzene / 40 h / 25 °C
3: 100 percent / tetra-n-butylammonium fluoride (TBAF) / tetrahydrofuran / 0.33 h / 20 °C
4: 99 percent / m-CPBA / CH2Cl2 / 1 h / 25 °C
With
18-crown-6 ether; tetrabutyl ammonium fluoride; caesium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; acetonitrile; benzene;
DOI:10.1021/ja00049a022
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 90 percent / triethylamine / CH2Cl2 / 0.5 h / 20 °C
2: 100 percent / DMAP / CH2Cl2 / 48 h / 25 °C
3: 95 percent / n-Bu3SnH, AIBN / benzene / 1 h / 70 °C
4: cesium carbonate, 18-crown-6 / acetonitrile / 40 h / 25 °C
5: acetonitrile; benzene / 40 h / 25 °C
6: 100 percent / tetra-n-butylammonium fluoride (TBAF) / tetrahydrofuran / 0.33 h / 20 °C
7: 99 percent / m-CPBA / CH2Cl2 / 1 h / 25 °C
With
dmap; 18-crown-6 ether; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; caesium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; acetonitrile; benzene;
DOI:10.1021/ja00049a022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetonitrile; benzene / 40 h / 25 °C
2: 100 percent / tetra-n-butylammonium fluoride (TBAF) / tetrahydrofuran / 0.33 h / 20 °C
3: 99 percent / m-CPBA / CH2Cl2 / 1 h / 25 °C
With
tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; acetonitrile; benzene;
DOI:10.1021/ja00049a022