(1Z,3E)-1-dimethylphenylsilyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-decadiene

Base Information

Chemical Name:(1Z,3E)-1-dimethylphenylsilyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-decadiene
CAS No.:339166-96-0
Molecular Formula:C₂₄H₃₉BO₂Si
Molecular Weight:398.469
Hs Code.:

Synonyms:(1Z,3E)-1-dimethylphenylsilyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-decadiene

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Chemical Property of (1Z,3E)-1-dimethylphenylsilyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-decadiene

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Technology Process of (1Z,3E)-1-dimethylphenylsilyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-decadiene

There total 1 articles about (1Z,3E)-1-dimethylphenylsilyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-decadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 96251-47-7
(1E,3E)-1-chloro-1,3-decadiene

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 339166-96-0
(1Z,3E)-1-dimethylphenylsilyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-decadiene

Guidance literature:: (1E,3E)-1-chloro-1,3-decadiene; With n-butyllithium; In tetrahydrofuran; hexane; at -90 ℃; for 0.25h;

dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane; In tetrahydrofuran; hexane; at -90 - 20 ℃;
DOI:10.1002/1521-3773(20010216)40:4<790::AID-ANIE7900>3.0.CO;2-T

Reference yield: 99.0%

: 932-87-6
1-Bromo-2-phenylacetylene

: 339166-96-0
(1Z,3E)-1-dimethylphenylsilyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-decadiene

: (3Z,5E)-3-dimethylphenylsilyl-1-phenyldodeca-3,5-dien-1-yne

Guidance literature:: With potassium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 90 ℃; for 12h;
DOI:10.1016/S0040-4020(02)00648-8

Reference yield: 94.0%

: 591-50-4
iodobenzene

: 339166-96-0
(1Z,3E)-1-dimethylphenylsilyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-decadiene

: (1Z,3E)-1-dimethylphenylsilyl-1-phenyl-1,3-decadiene

Guidance literature:: With potassium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 90 ℃; for 12h;
DOI:10.1016/S0040-4020(02)00648-8