(4-bromophenyl)formamido 2,2-dimethylpropanoate

Base Information

Chemical Name:(4-bromophenyl)formamido 2,2-dimethylpropanoate
CAS No.:1352801-45-6
Molecular Formula:C₁₂H₁₄BrNO₃
Molecular Weight:300.152
Hs Code.:

Synonyms:(4-bromophenyl)formamido 2,2-dimethylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-bromophenyl)formamido 2,2-dimethylpropanoate

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Technology Process of (4-bromophenyl)formamido 2,2-dimethylpropanoate

There total 4 articles about (4-bromophenyl)formamido 2,2-dimethylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1293990-73-4
O-pivaloylhydroxylamine trifluoromethanesulfonate salt

: 586-75-4
4-chlorobenzoyl chloride

: 1352801-45-6
(4-bromophenyl)formamido 2,2-dimethylpropanoate

Guidance literature:: With potassium carbonate; In water; ethyl acetate; at 0 - 20 ℃;
DOI:10.1021/ja5072702

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 1352801-45-6
(4-bromophenyl)formamido 2,2-dimethylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

2.1: sodium carbonate / water; ethyl acetate / 20 °C / Inert atmosphere

2.2: 4 h / 0 - 20 °C / Inert atmosphere

With oxalyl dichloride; sodium carbonate; N,N-dimethyl-formamide; In dichloromethane; water; ethyl acetate;
DOI:10.1021/ol203353a