6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl}-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylic acid

Base Information

Chemical Name:6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl}-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylic acid
CAS No.:1007170-18-4
Molecular Formula:C₂₅H₂₇ClN₂O₅
Molecular Weight:470.953
Hs Code.:

Synonyms:6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl}-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylic acid

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Chemical Property of 6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl}-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylic acid

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Technology Process of 6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl}-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylic acid

There total 1 articles about 6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl}-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1007170-17-3
ethyl 6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl)-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylate

: 1007170-18-4
6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl}-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylic acid

Guidance literature:: ethyl 6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl)-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylate; With ethanol; potassium hydroxide; for 2h; Reflux;

With hydrogenchloride; In ethanol; water;

Reference yield: 41.0%

: 1007170-18-4
6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl}-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylic acid

: 2756-85-6
1-aminocyclohexane carboxylic acid

: 1-({[6-{4-chloro-3-{3-(dimethylamino)propoxy]phenyl}-5-(2,6-dimethoxyphenyl)pyridin-2-yl]carbonyl}amino)cyclohexanecarboxylic acid hydrochloride

Guidance literature:: 1-aminocyclohexane carboxylic acid; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 90 ℃; for 2h; Inert atmosphere;

6-{4-chloro-3-[3-(dimethylamino)propoxy]phenyl}-5-(2,6-dimethoxyphenyl)pyridine-2-carboxylic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃; for 18h; Inert atmosphere;

With hydrogenchloride; In water; N,N-dimethyl-formamide; acetonitrile; for 3h;