m-Nitrophenylmaleic anhydride

Base Information

• Chemical Name: m-Nitrophenylmaleic anhydride
• CAS No.: 108655-18-1
• Molecular Formula: C₁₀H₅NO₅
• Molecular Weight: 219.153
• Mol file: 108655-18-1.mol

Synonyms:m-Nitrophenylmaleic anhydride

Chemical Property of m-Nitrophenylmaleic anhydride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of m-Nitrophenylmaleic anhydride

There total 3 articles about m-Nitrophenylmaleic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

3-(3-nitrophenyl)dihydrofuran-2,5-dione (108655-17-0) → m-Nitrophenylmaleic anhydride (108655-18-1)

Guidance literature:

With N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; for 26h; Heating;

DOI:10.1007/BF00522738

Reference yield:

3-cyano-3-(3-nitrophenyl)-acrylic acid potassium salt (333792-64-6) → m-Nitrophenylmaleic anhydride (108655-18-1)

Guidance literature:

With sulfuric acid; water; In formic acid; for 3h; Heating / reflux;

Reference yield:

2-(3-nitrophenyl)succinic acid (69006-92-4) → m-Nitrophenylmaleic anhydride (108655-18-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / Acetyl chloride, Thionylchloride / Heating

2: 38 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 26 h / Heating

With N-Bromosuccinimide; thionyl chloride; Perbenzoic acid; acetyl chloride; In tetrachloromethane;

DOI:10.1007/BF00522738

upstream raw materials:

3-(3-nitrophenyl)dihydrofuran-2,5-dione

2-(3-nitrophenyl)succinic acid

3-cyano-3-(3-nitrophenyl)-acrylic acid potassium salt

Downstream raw materials:

4-(m-Nitrophenyl)-3,6-dioxo-1,2,3,6-tetrahydropyridazine