{4-[4-benzyloxy-6-(4-hydroxymethyl-phenylsulfanylmethyl)-pyridin-2-ylmethylsulfanyl]-phenyl}-methanol

Base Information

Chemical Name:{4-[4-benzyloxy-6-(4-hydroxymethyl-phenylsulfanylmethyl)-pyridin-2-ylmethylsulfanyl]-phenyl}-methanol
CAS No.:231955-90-1
Molecular Formula:C₂₈H₂₇NO₃S₂
Molecular Weight:489.659
Hs Code.:

Synonyms:{4-[4-benzyloxy-6-(4-hydroxymethyl-phenylsulfanylmethyl)-pyridin-2-ylmethylsulfanyl]-phenyl}-methanol

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Chemical Property of {4-[4-benzyloxy-6-(4-hydroxymethyl-phenylsulfanylmethyl)-pyridin-2-ylmethylsulfanyl]-phenyl}-methanol

Chemical Property:

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Technology Process of {4-[4-benzyloxy-6-(4-hydroxymethyl-phenylsulfanylmethyl)-pyridin-2-ylmethylsulfanyl]-phenyl}-methanol

There total 1 articles about {4-[4-benzyloxy-6-(4-hydroxymethyl-phenylsulfanylmethyl)-pyridin-2-ylmethylsulfanyl]-phenyl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53339-53-0
4-mercaptobenzyl alcohol

: 171000-40-1
4-(benzyloxy)-2,6-bis(chloromethyl)pyridine

: 231955-90-1
{4-[4-benzyloxy-6-(4-hydroxymethyl-phenylsulfanylmethyl)-pyridin-2-ylmethylsulfanyl]-phenyl}-methanol

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 24h;
DOI:10.1039/a900783k

Reference yield:

: 231955-90-1
{4-[4-benzyloxy-6-(4-hydroxymethyl-phenylsulfanylmethyl)-pyridin-2-ylmethylsulfanyl]-phenyl}-methanol

: 231955-91-2
4-benzyloxy-2,6-bis-(4-chloromethyl-phenylsulfanylmethyl)-pyridine

Guidance literature:: With thionyl chloride; at 50 ℃; for 4h;
DOI:10.1039/a900783k

Reference yield:

: 231955-90-1
{4-[4-benzyloxy-6-(4-hydroxymethyl-phenylsulfanylmethyl)-pyridin-2-ylmethylsulfanyl]-phenyl}-methanol

: 231955-82-1
C₆H₅CH₂OC₅NH₂[CH₂SC₆H₄CH₂OC₅NH₂(COOC₂H₅)2]2

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 4 h / 50 °C

2: 92 percent / K₂CO₃ / dimethylformamide / 24 h / 70 °C

With thionyl chloride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/a900783k