DW₂₂₈₂-N-Boc-L-Ala

Base Information

• Chemical Name: DW₂₂₈₂-N-Boc-L-Ala
• CAS No.: 203861-21-6
• Molecular Formula: C₃₂H₃₅N₅O₇S
• Molecular Weight: 633.725
• Mol file: 203861-21-6.mol

Synonyms:DW₂₂₈₂-N-Boc-L-Ala

Chemical Property of DW₂₂₈₂-N-Boc-L-Ala

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of DW₂₂₈₂-N-Boc-L-Ala

There total 1 articles about DW₂₂₈₂-N-Boc-L-Ala which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.1%

L-N-Boc-Ala (15761-38-3) + (4S)-1-[1-(4-aminobenzoyl)-2,3-dihydro-1H-indol-6-sulfonyl]-4-phenylimidazolidin-2-one → DW2282-N-Boc-L-Ala (203861-21-6)

Guidance literature:

(4S)-1-[1-(4-aminobenzoyl)-2,3-dihydro-1H-indol-6-sulfonyl]-4-phenylimidazolidin-2-one; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

L-N-Boc-Ala; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h;

DOI:10.1016/j.ejmech.2014.04.048

Reference yield: 70.6%

DW2282-N-Boc-L-Ala (203861-21-6) + trifluoroacetic acid (76-05-1) → DW2282-Ala*TFA

Guidance literature:

In dichloromethane; at 20 ℃; for 3h;

DOI:10.1016/j.ejmech.2014.04.048

upstream raw materials:

L-N-Boc-Ala