C₂₅H₃₆O₃Si

Base Information

Chemical Name:C₂₅H₃₆O₃Si
CAS No.:1384271-71-9
Molecular Formula:C₂₅H₃₆O₃Si
Molecular Weight:412.645
Hs Code.:

C<sub>25</sub>H<sub>36</sub>O<sub>3</sub>Si

Synonyms:C₂₅H₃₆O₃Si

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Chemical Property of C₂₅H₃₆O₃Si

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Technology Process of C₂₅H₃₆O₃Si

There total 7 articles about C₂₅H₃₆O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1384271-72-0
C₂₅H₃₄O₂Si

: 1384271-71-9
C₂₅H₃₆O₃Si

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; water; at 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2012.04.118

Reference yield:

: 1384271-73-1
C₁₃H₂₂O₃

: 1384271-71-9
C₂₅H₃₆O₃Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1H-imidazole / dichloromethane / 0 - 20 °C

2.1: methanol; toluene-4-sulfonic acid / 0 - 20 °C

3.1: sodium tetrahydroborate; nickel diacetate / ethanol; ethylene glycol / 6 h / 20 °C

4.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 12 h / -20 °C / Molecular sieve

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

5.2: -78 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 - 20 °C

7.1: scandium tris(trifluoromethanesulfonate) / tetrahydrofuran; water / 12 h / 20 °C

With 1H-imidazole; titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; sodium tetrahydroborate; oxalyl dichloride; L-(+)-diisopropyl tartrate; sodium hexamethyldisilazane; nickel diacetate; toluene-4-sulfonic acid; dimethyl sulfoxide; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; ethanol; dichloromethane; water; ethylene glycol; 4.1: Sharpless epoxidation / 5.1: Swern oxidation / 5.2: Swern oxidation;
DOI:10.1016/j.tetlet.2012.04.118

Reference yield:

: 1384271-75-3
C₂₉H₄₀O₃Si

: 1384271-71-9
C₂₅H₃₆O₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanol; toluene-4-sulfonic acid / 0 - 20 °C

2.1: sodium tetrahydroborate; nickel diacetate / ethanol; ethylene glycol / 6 h / 20 °C

3.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 12 h / -20 °C / Molecular sieve

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

4.2: -78 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 - 20 °C

6.1: scandium tris(trifluoromethanesulfonate) / tetrahydrofuran; water / 12 h / 20 °C

With titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; sodium tetrahydroborate; oxalyl dichloride; L-(+)-diisopropyl tartrate; sodium hexamethyldisilazane; nickel diacetate; toluene-4-sulfonic acid; dimethyl sulfoxide; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; ethanol; dichloromethane; water; ethylene glycol; 3.1: Sharpless epoxidation / 4.1: Swern oxidation / 4.2: Swern oxidation;
DOI:10.1016/j.tetlet.2012.04.118