C₅₆H₆₀N₂O₇

Base Information

• Chemical Name: C₅₆H₆₀N₂O₇
• CAS No.: 1413373-64-4
• Molecular Formula: C₅₆H₆₀N₂O₇
• Molecular Weight: 873.102
• Mol file: 1413373-64-4.mol

Synonyms:C₅₆H₆₀N₂O₇

Chemical Property of C₅₆H₆₀N₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₆H₆₀N₂O₇

There total 19 articles about C₅₆H₆₀N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

C56H58N2O6 (1413373-62-2) → C56H60N2O7 (1413373-64-4)

Guidance literature:

C₅₆H₅₈N₂O₆; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; Inert atmosphere; Reflux;

With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; at 0 ℃; for 3h;

Reference yield:

2,3,4,6-Tetra-O-benzyl-D-glucopyranose (4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9) → C56H60N2O7 (1413373-64-4)

Guidance literature:

Multi-step reaction with 8 steps

1.1: toluene; tetrahydrofuran / 3.67 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - 20 °C

3.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

4.1: pyridine; trichlorophosphate / 0 - 20 °C

5.1: L-Selectride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

5.2: 0.25 h

6.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / tetrahydrofuran / 30 °C / Inert atmosphere

7.1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

8.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / Inert atmosphere; Reflux

8.2: 3 h / 0 °C

With pyridine; oxalyl dichloride; tributylphosphine; L-Selectride; caesium carbonate; dimethyl sulfoxide; 9-bora-bicyclo[3.3.1]nonane; L-proline; 1,1'-azodicarbonyl-dipiperidine; trichlorophosphate; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 6.1: Mitsunobu reaction;

Reference yield:

(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one (13096-62-3) → C56H60N2O7 (1413373-64-4)

Guidance literature:

Multi-step reaction with 8 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 0 °C

1.3: cooling with ice

2.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C

3.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

3.2: -78 - 0 °C

4.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C

5.1: L-Selectride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

5.2: 0.25 h

6.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / tetrahydrofuran / 30 °C / Inert atmosphere

7.1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

8.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / Inert atmosphere; Reflux

8.2: 3 h / 0 °C

With sodium tetrahydroborate; n-butyllithium; tributylphosphine; L-Selectride; potassium carbonate; caesium carbonate; dimethyl sulfoxide; 9-bora-bicyclo[3.3.1]nonane; trifluoroacetic anhydride; 1,1'-azodicarbonyl-dipiperidine; 18-crown-6 ether; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; 6.1: Mitsunobu reaction;

upstream raw materials:

benzyl bromide

4-benzyloxybenzyl alcohol

4-hydroxy-benzaldehyde

2,3,4,6-Tetra-O-benzyl-D-glucopyranose

Downstream raw materials:

C₅₆H₅₈F₂N₂O₆

Refernces