4-[(4,5-Dihydroxy-10-oxo-9,10-dihydro-anthracen-9-yl)-methoxy-methyl]-benzonitrile

Base Information

Chemical Name:4-[(4,5-Dihydroxy-10-oxo-9,10-dihydro-anthracen-9-yl)-methoxy-methyl]-benzonitrile
CAS No.:151562-83-3
Molecular Formula:C₂₃H₁₇NO₄
Molecular Weight:371.392
Hs Code.:

Synonyms:4-[(4,5-Dihydroxy-10-oxo-9,10-dihydro-anthracen-9-yl)-methoxy-methyl]-benzonitrile

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Chemical Property of 4-[(4,5-Dihydroxy-10-oxo-9,10-dihydro-anthracen-9-yl)-methoxy-methyl]-benzonitrile

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Technology Process of 4-[(4,5-Dihydroxy-10-oxo-9,10-dihydro-anthracen-9-yl)-methoxy-methyl]-benzonitrile

There total 3 articles about 4-[(4,5-Dihydroxy-10-oxo-9,10-dihydro-anthracen-9-yl)-methoxy-methyl]-benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1143-38-0
1,8-dihydroxy-9(10H)-anthracenone

: 162750-64-3
4-(Chloro-methoxy-methyl)-benzonitrile

: 151562-83-3
4-[(4,5-Dihydroxy-10-oxo-9,10-dihydro-anthracen-9-yl)-methoxy-methyl]-benzonitrile

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 0.5h; Yield given;
DOI:10.1021/jm00077a015

Reference yield:

: 90921-71-4
4-(dimethoxymethyl)benzonitrile

: 151562-83-3
4-[(4,5-Dihydroxy-10-oxo-9,10-dihydro-anthracen-9-yl)-methoxy-methyl]-benzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride, thionyl chloride / 50 - 60 °C

2: 1,8-diazabicyclo<5.4.0>undec-7-ene / CH₂Cl₂ / 0.5 h / 0 °C

With thionyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; acetyl chloride; In dichloromethane;
DOI:10.1021/jm00077a015

Reference yield:

: 105-07-7
4-cyanobenzaldehyde

: 151562-83-3
4-[(4,5-Dihydroxy-10-oxo-9,10-dihydro-anthracen-9-yl)-methoxy-methyl]-benzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄ / methanol

2: acetyl chloride, thionyl chloride / 50 - 60 °C

3: 1,8-diazabicyclo<5.4.0>undec-7-ene / CH₂Cl₂ / 0.5 h / 0 °C

With thionyl chloride; sulfuric acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; acetyl chloride; In methanol; dichloromethane;
DOI:10.1021/jm00077a015