C₂₅H₃₄O₆

Base Information

Chemical Name:C₂₅H₃₄O₆
CAS No.:1263144-06-4
Molecular Formula:C₂₅H₃₄O₆
Molecular Weight:430.541
Hs Code.:

C<sub>25</sub>H<sub>34</sub>O<sub>6</sub>

Synonyms:C₂₅H₃₄O₆

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Chemical Property of C₂₅H₃₄O₆

Chemical Property:

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Technology Process of C₂₅H₃₄O₆

There total 5 articles about C₂₅H₃₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1263144-20-2
C₄₀H₆₈O₆Si₂

: 1263144-06-4
C₂₅H₃₄O₆

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 - 50 ℃; for 2.5h;
DOI:10.1016/j.tet.2010.11.017

Reference yield:

: 835882-70-7
(2R)-6-(tert-butyldimethylsilanyloxy)-1-trityloxyhex-4-yn-2-ol

: 1263144-06-4
C₂₅H₃₄O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: silver nitrate; triethylamine / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C

1.2: 12 h / 0 - 20 °C

2.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 3.33 h / -78 - -20 °C

3.1: quinoline; hydrogen / ethyl acetate / 2 h / 20 °C

4.1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / 4 h / 20 °C

5.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.83 h / 0 °C

6.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 8 h / 0 - 20 °C

7.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; ((diphenylphosphoryl)oxy)copper(I); triethyl phosphite / tetrahydrofuran; hexane / 20 °C

8.1: cerium(III) chloride heptahydrate / ethanol / 0.33 h / 20 °C

8.2: 1.5 h / -40 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.5 h / 20 - 50 °C

With quinoline; triethylsilane; sodium chlorite; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium dihydrogenphosphate; 2-methyl-but-2-ene; ((diphenylphosphoryl)oxy)copper(I); cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; silver nitrate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; triethyl phosphite; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol; 7.1: Stille-type coupling;
DOI:10.1016/j.tet.2010.11.017

Reference yield:

: 1263144-28-0
C₁₂H₂₄O₃Si

: 1263144-06-4
C₂₅H₃₄O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: dmap; triethylamine / 9.5 h / 20 °C

2.1: silver nitrate; triethylamine / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C

2.2: 12 h / 0 - 20 °C

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 3.33 h / -78 - -20 °C

4.1: quinoline; hydrogen / ethyl acetate / 2 h / 20 °C

5.1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / 4 h / 20 °C

6.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.83 h / 0 °C

7.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 8 h / 0 - 20 °C

8.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; ((diphenylphosphoryl)oxy)copper(I); triethyl phosphite / tetrahydrofuran; hexane / 20 °C

9.1: cerium(III) chloride heptahydrate / ethanol / 0.33 h / 20 °C

9.2: 1.5 h / -40 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.5 h / 20 - 50 °C

With quinoline; triethylsilane; dmap; sodium chlorite; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium dihydrogenphosphate; 2-methyl-but-2-ene; ((diphenylphosphoryl)oxy)copper(I); cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; silver nitrate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; triethyl phosphite; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol; 8.1: Stille-type coupling;
DOI:10.1016/j.tet.2010.11.017