1-(2,6-dimethylphenyl)-4,4-diphenyl-2-(methylamino)-2-imidazoline-5-thione

Base Information

• Chemical Name: 1-(2,6-dimethylphenyl)-4,4-diphenyl-2-(methylamino)-2-imidazoline-5-thione
• CAS No.: 118515-03-0
• Molecular Formula: C₂₄H₂₃N₃S
• Molecular Weight: 385.533

Synonyms:1-(2,6-dimethylphenyl)-4,4-diphenyl-2-(methylamino)-2-imidazoline-5-thione

Chemical Property of 1-(2,6-dimethylphenyl)-4,4-diphenyl-2-(methylamino)-2-imidazoline-5-thione

Chemical Property:

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Technology Process of 1-(2,6-dimethylphenyl)-4,4-diphenyl-2-(methylamino)-2-imidazoline-5-thione

There total 6 articles about 1-(2,6-dimethylphenyl)-4,4-diphenyl-2-(methylamino)-2-imidazoline-5-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(2,6-Dimethyl-phenyl)-[2-methylamino-4,4-diphenyl-4H-thiazol-(5Z)-ylidene]-amine (118515-10-9) → 1-(2,6-dimethylphenyl)-4,4-diphenyl-2-(methylamino)-2-imidazoline-5-thione (118515-03-0)

Guidance literature:

With 2,6-dichloro-benzonitrile; In acetonitrile; for 2h; Heating;

DOI:10.1021/jo00293a011

Reference yield: 10.0%

1-Benzhydrylidene-3-methyl-thiourea (34979-85-6) + 2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) → (2,6-Dimethyl-phenyl)-[2-methylamino-4,4-diphenyl-4H-thiazol-(5Z)-ylidene]-amine (118515-10-9) + 1-(2,6-dimethylphenyl)-4,4-diphenyl-2-(methylamino)-2-imidazoline-5-thione (118515-03-0)

Guidance literature:

In tetrahydrofuran; for 360h; Heating;

DOI:10.1021/jo00293a011

Reference yield: 7.0%

2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) + 1-Benzhydrylidene-2,3-dimethyl-isothiourea; hydriodide (118514-71-9) → 1-(2,6-dimethylphenyl)-4,4-diphenyl-2-(methylamino)-2-imidazoline-5-thione (118515-03-0) + 4,5-dihydro-5-<(2,6-dimethylphenyl)imino>-4,4-diphenyl-2-(methylamino)thiazole (118515-10-9) + 5-<(2,6-dimethylphenyl)imino>-4,4-diphenyl-1-methyl-2-(methylthio)-2-imidazoline (118514-89-9)

Guidance literature:

In acetonitrile; for 3h; Heating;

DOI:10.1021/jo00266a035

upstream raw materials:

1-Benzhydrylidene-3-methyl-thiourea

2,6-dimethylphenyl isonitrile

1-Benzhydrylidene-2,3-dimethyl-isothiourea; hydriodide

(2,6-Dimethyl-phenyl)-[2-methylamino-4,4-diphenyl-4H-thiazol-(5Z)-ylidene]-amine

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