[(acetylacetonate)2Ru(μ-3,6-bis(2'-pyridyl)pyridazine-H(+))Ru(acetylacetonate)2](ClO4)

Base Information

Chemical Name:[(acetylacetonate)2Ru(μ-3,6-bis(2'-pyridyl)pyridazine-H(+))Ru(acetylacetonate)2](ClO4)
CAS No.:849337-67-3
Molecular Formula:C₃₄H₃₇N₄O₈Ru₂*ClO₄
Molecular Weight:931.28
Hs Code.:

Synonyms:[(acetylacetonate)2Ru(μ-3,6-bis(2'-pyridyl)pyridazine-H(+))Ru(acetylacetonate)2](ClO4)

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Chemical Property of [(acetylacetonate)2Ru(μ-3,6-bis(2'-pyridyl)pyridazine-H(+))Ru(acetylacetonate)2](ClO4)

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Technology Process of [(acetylacetonate)2Ru(μ-3,6-bis(2'-pyridyl)pyridazine-H(+))Ru(acetylacetonate)2](ClO4)

There total 1 articles about [(acetylacetonate)2Ru(μ-3,6-bis(2'-pyridyl)pyridazine-H(+))Ru(acetylacetonate)2](ClO4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: bis(acetonitrile)bis(2,4-pentanedionato)ruthenium(II)

: sodium perchlorate

: 36901-11-8
3,6-di(pyridin-2'-yl)-s-tetrazine

: 31378-26-4,31378-27-5,14284-93-6
tris(2,4-pentanedionato)ruthenium(III)

: 849337-64-0
(acetylacetonate)2Ru(3,6-bis(2'-pyridyl)pyridazine)

: 849337-67-3
[(acetylacetonate)2Ru(μ-3,6-bis(2'-pyridyl)pyridazine-H(+))Ru(acetylacetonate)2](ClO4)

Guidance literature:: In ethanol; water; acetonitrile; under N2; soln. of Ru-contg. compd. (0.26 mmol) and ligand (0.13 mmol) in EtOH was heated to reflux for 6 h; mixt. was evapd. to dryness; solid obtained was dissolved in min. vol. of CH3CN; aq. soln. of NaClO4 was added; keeping at 0°C overnight; the mixt. was filtered, ppt. was washed with cold ethanol, and dried under vac.; purifn. with alumina column; elution with CH2Cl2-CH3CN; evapn. of the solvent under reduced pressure; elem. anal.;
DOI:10.1039/b417530a