1-<(3,4-dichlorophenyl)methyl>-5,6-dimethyl-2,4(1H,3H)-pyrimidinedione

Base Information

Chemical Name:1-<(3,4-dichlorophenyl)methyl>-5,6-dimethyl-2,4(1H,3H)-pyrimidinedione
CAS No.:133167-04-1
Molecular Formula:C₁₃H₁₂Cl₂N₂O₂
Molecular Weight:299.156
Hs Code.:

Synonyms:1-<(3,4-dichlorophenyl)methyl>-5,6-dimethyl-2,4(1H,3H)-pyrimidinedione

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Chemical Property of 1-<(3,4-dichlorophenyl)methyl>-5,6-dimethyl-2,4(1H,3H)-pyrimidinedione

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Technology Process of 1-<(3,4-dichlorophenyl)methyl>-5,6-dimethyl-2,4(1H,3H)-pyrimidinedione

There total 1 articles about 1-<(3,4-dichlorophenyl)methyl>-5,6-dimethyl-2,4(1H,3H)-pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.1%

: 61736-31-0
5,6-dimethyl-2H,4H-1,3-oxazine-2,4-dione

: 102-49-8
3,4-dichlorobenzyl amine

: 133167-04-1
1-<(3,4-dichlorophenyl)methyl>-5,6-dimethyl-2,4(1H,3H)-pyrimidinedione

Guidance literature:: In ethanol; at 110 ℃; for 1.5h;
DOI:10.1021/jm00108a038

Reference yield: 76.6%

: 133167-04-1
1-<(3,4-dichlorophenyl)methyl>-5,6-dimethyl-2,4(1H,3H)-pyrimidinedione

: 96-32-2
bromoacetic acid methyl ester

: 133167-05-2
3-<(3,4-dichlorophenyl)methyl>-3,6-dihydro-4,5-dimethyl-2,6-dioxo-1(2H)-pyrimidineacetic acid methyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 4h;
DOI:10.1021/jm00108a038

Reference yield:

: 133167-04-1
1-<(3,4-dichlorophenyl)methyl>-5,6-dimethyl-2,4(1H,3H)-pyrimidinedione

: 133166-79-7
3-<(3,4-dichlorophenyl)methyl>-3,6-dihydro-4,5-dimethyl-2,6-dioxo-1(2H)-pyrimidineacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 76.6 percent / K₂CO₃ / dimethylformamide / 4 h / 60 °C

2: 77 percent / 2.5 N aq. NaOH / methanol; tetrahydrofuran / 1 h

With sodium hydroxide; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00108a038