C₁₉H₂₀O₆

Base Information

• Chemical Name: C₁₉H₂₀O₆
• CAS No.: 916053-77-5
• Molecular Formula: C₁₉H₂₀O₆
• Molecular Weight: 344.364
• Mol file: 916053-77-5.mol

Synonyms:C₁₉H₂₀O₆

Chemical Property of C₁₉H₂₀O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₂₀O₆

There total 2 articles about C₁₉H₂₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C38H55NO6Si2 → C19H20O6 (916053-77-5)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 40 - 50 ℃;

DOI:10.1055/s-2006-948168

Reference yield:

1-(benzyloxy)-4-(chloromethyl)-2-methoxybenzene (33688-50-5) → C19H20O6 (916053-77-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran

1.2: 64 percent / tetrahydrofuran

2.1: 100 percent / aq. HCl / dioxane / 40 - 50 °C

With hydrogenchloride; magnesium; In tetrahydrofuran; 1,4-dioxane;

DOI:10.1055/s-2006-948168

Reference yield:

C19H20O6 (916053-77-5) → C35H38O5Si (916053-80-0)

Guidance literature:

Multi-step reaction with 3 steps

1: DMAP; pyridine / acetonitrile

2: Bu₃SnH; AIBN / toluene / Heating

3: 81 percent / imidazole / CH₂Cl₂

With pyridine; 1H-imidazole; dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In dichloromethane; toluene; acetonitrile;

DOI:10.1055/s-2006-948168

upstream raw materials:

1-(benzyloxy)-4-(chloromethyl)-2-methoxybenzene

Downstream raw materials:

C₃₅H₃₈O₅Si

C₁₉H₂₀O₅

C₂₆H₂₆O₅