4-[bis(4-bromophenyl)amino]benzyltriethylammonium trifluoromethanesulfonate

Base Information

Chemical Name:4-[bis(4-bromophenyl)amino]benzyltriethylammonium trifluoromethanesulfonate
CAS No.:1392835-20-9
Molecular Formula:CF₃O₃S*C₂₅H₂₉Br₂N₂
Molecular Weight:666.397
Hs Code.:

Synonyms:4-[bis(4-bromophenyl)amino]benzyltriethylammonium trifluoromethanesulfonate

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Chemical Property of 4-[bis(4-bromophenyl)amino]benzyltriethylammonium trifluoromethanesulfonate

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Technology Process of 4-[bis(4-bromophenyl)amino]benzyltriethylammonium trifluoromethanesulfonate

There total 3 articles about 4-[bis(4-bromophenyl)amino]benzyltriethylammonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 421-83-0
trifluoromethane sulfonyl chloride

: 536992-67-3
(4-(bis(4-bromophenyl)amino)-phenyl)methanol

: 121-44-8
triethylamine

: 1392835-20-9
4-[bis(4-bromophenyl)amino]benzyltriethylammonium trifluoromethanesulfonate

Guidance literature:: In dichloromethane; at 0 ℃; for 2h;
DOI:10.1016/j.electacta.2012.05.049

Reference yield:

: 81090-53-1
N,N-bis(4-bromophenyl)aniline

: 1392835-20-9
4-[bis(4-bromophenyl)amino]benzyltriethylammonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 1 h / 95 °C

1.2: 0.5 h

2.1: sodium tetrahydroborate; sodium hydroxide / tetrahydrofuran; ethanol / 1 h / 20 °C

3.1: dichloromethane / 2 h / 0 °C

With sodium tetrahydroborate; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane; 1.1: Vilsmeier-Haack reaction;
DOI:10.1016/j.electacta.2012.05.049

Reference yield:

: 25069-38-9
N,N-bis(4-bromophenyl)aminobenzaldehyde

: 1392835-20-9
4-[bis(4-bromophenyl)amino]benzyltriethylammonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; sodium hydroxide / tetrahydrofuran; ethanol / 1 h / 20 °C

2: dichloromethane / 2 h / 0 °C

With sodium tetrahydroborate; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.electacta.2012.05.049